Time Resolved in situ X-Ray Tomographic Microscopy Unraveling Dynamic Processes in Geologic Systems

Marone, Federica; Marti, Sina; Fußeis, Florian; Velásquez-Parra, Andrés; Griffa, Michele; Jiménez‐Martínez, Joaquín; Dobson, Katherine J.; Stampanoni, Marco

doi:10.3389/feart.2019.00346

Cited by 32 publications

(37 citation statements)

References 83 publications

(96 reference statements)

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“…Several synchrotron facilities now have the capability to acquire 3D images of geological materials with moderate (10-5 µm) or high (<5 µm) spatial resolution. Several tomography beamlines can achieve fast (defined here as <10 s to collect a single 3D tomographic dataset) tomography of these samples, and those focusing on imaging dynamic systems can routinely perform ultra-fast or real-time (defined here as <1 s to collect a single 3D tomographic dataset) tomography on geological specimens (e.g., Marone et al, 2020). For 3D tomographic acquisition, a frequency of up to 20 tomographies per second (TPS) is now possible (Dobson et al, 2016).…”

Section: Recent Advances In Synchrotron Capabilitymentioning

confidence: 99%

“…Data transfer, rather than experimental speed, is now often the bottleneck. This has led to investment in novel continuous read out detectors with real-time data transfer to network storage (Mokso et al, 2017;Marone et al, 2020), and at some beamlines there is no theoretical limit to the number of 3D datasets that can be obtained.…”

Section: Recent Advances In Synchrotron Capabilitymentioning

confidence: 99%

“…To achieve the fastest projection acquisition rates for realtime or ultra-fast synchrotron tomography, magmatic sample densities may limit users to a white or pink beam on the lower energy hard X-ray imaging beamlines (e.g., TOMCAT, Swiss Light Source; Marone et al, 2020), but still allow monochromatic imaging on higher energy beamlines (e.g., i12-JEEP, Diamond Light Source; Drakopoulos et al, 2015). The attenuation differences between most rock-forming minerals are greatest at lower energies (Hanna and Ketcham, 2017).…”

Section: Imaging Moving Magmamentioning

confidence: 99%

“…At TOMCAT (SLS) the XRheo is compatible with the laser heating system (Figure 1; Fife et al, 2012;Marone et al, 2020). This system has two lasers mounted on opposite sides of the sample, each generating a 6 mm × 4 mm portrait spot on the sample holder.…”

Section: Working At Magmatic Temperatures On Synchrotron Beamlinesmentioning

confidence: 99%

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Quantifying Microstructural Evolution in Moving Magma

et al. 2020

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Many of the grand challenges in volcanic and magmatic research are focused on understanding the dynamics of highly heterogeneous systems and the critical conditions that enable magmas to move or eruptions to initiate. From the formation and development of magma reservoirs, through propagation and arrest of magma, to the conditions in the conduit, gas escape, eruption dynamics, and beyond into the environmental impacts of that eruption, we are trying to define how processes occur, their rates and timings, and their causes and consequences. However, we are usually unable to observe the processes directly. Here we give a short synopsis of the new capabilities and highlight the potential insights that in situ observation can provide. We present the XRheo and Pele furnace experimental apparatus and analytical toolkit for the in situ X-ray tomography-based quantification of magmatic microstructural evolution during rheological testing. We present the first 3D data showing the evolving textural heterogeneity within a shearing magma, highlighting the dynamic changes to microstructure that occur from the initiation of shear, and the variability of the microstructural response to that shear as deformation progresses. The particular shear experiments highlighted here focus on the effect of shear on bubble coalescence with a view to shedding light on both magma transport and fragmentation processes. The XRheo system is intended to help us understand the microstructural controls on the complex and non-Newtonian evolution of magma rheology, and is therefore

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Section: Recent Advances In Synchrotron Capabilitymentioning

confidence: 99%

Section: Recent Advances In Synchrotron Capabilitymentioning

confidence: 99%

Section: Imaging Moving Magmamentioning

confidence: 99%

Section: Working At Magmatic Temperatures On Synchrotron Beamlinesmentioning

confidence: 99%

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Quantifying Microstructural Evolution in Moving Magma

et al. 2020

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“…Indeed, the non-destructive nature of X-ray imaging is a great asset in studying dynamic processes as they take place. This technique, often named 4D micro-CT, has been applied already in a large number of application areas, such as petrophysics [12,13] and geosciences [14,15]. Within 4D micro-CT, a great variety exists in temporal and spatial resolution.…”

Section: Introductionmentioning

confidence: 99%

In-Situ X-ray Imaging Of Sublimating Spin-Frozen Solutions

et al. 2020

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Spin-freeze-drying is a promising technique to enable long-term storage of pharmaceutical unit doses of aqueous drug solutions. To investigate the sublimation of the ice during the primary phase of freeze-drying, X-ray imaging can yield crucial temporally resolved information on the local dynamics. In this paper, we describe a methodology to investigate the sublimation front during single unit-dose freeze-drying using 4D in-situ X-ray imaging. Three spin-frozen samples of different solutions were imaged using this methodology and the process characteristics were analysed and reduced to two-dimensional feature maps.

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Tomoscopy: Time‐Resolved Tomography for Dynamic Processes in Materials

et al. 2021

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The structure and constitution of opaque materials can be studied with X‐ray imaging methods such as 3D tomography. To observe the dynamic evolution of their structure and the distribution of constituents, for example, during processing, heating, mechanical loading, etc., 3D imaging has to be fast enough. In this paper, the recent developments of time‐resolved X‐ray tomography that have led to what one now calls “tomoscopy” are briefly reviewed A novel setup is presented and applied that pushes temporal resolution down to just 1 ms, that is, 1000 tomograms per second (tps) are acquired, while maintaining spatial resolutions of micrometers and running experiments for minutes without interruption. Applications recorded at different acquisition rates ranging from 50 to 1000 tps are presented. The authors observe and quantify the immiscible hypermonotectic reaction of AlBi10 (in wt%) alloy and dendrite evolution in AlGe10 (in wt%) casting alloy during fast solidification. The combustion process and the evolution of the constituents are analyzed in a burning sparkler. Finally, the authors follow the structure and density of two metal foams over a long period of time and derive details of bubble formation and bubble ageing including quantitative analyses of bubble parameters with millisecond temporal resolution.

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Time Resolved in situ X-Ray Tomographic Microscopy Unraveling Dynamic Processes in Geologic Systems

Cited by 32 publications

References 83 publications

Quantifying Microstructural Evolution in Moving Magma

Quantifying Microstructural Evolution in Moving Magma

In-Situ X-ray Imaging Of Sublimating Spin-Frozen Solutions

Tomoscopy: Time‐Resolved Tomography for Dynamic Processes in Materials

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