2007
DOI: 10.1007/s10965-007-9156-0
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Tragacanth gum-graft-polyacrylonitrile: synthesis, characterization and hydrolysis

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Cited by 77 publications
(30 citation statements)
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“…WA was measured by the tea‐bag method. This method is the most conventional, fast, and suitable for limited amount of samples 15, 16. The accurately weighted samples ( m 0 = 0.2 g) were placed into plastic bags (with fine meshes) and the bags were immersed into 500 mL of distilled water and saline solution (0.9 wt % NaCl aqueous solution) to reach the equilibrium swelling at room temperature (25°C), respectively.…”
Section: Methodsmentioning
confidence: 99%
“…WA was measured by the tea‐bag method. This method is the most conventional, fast, and suitable for limited amount of samples 15, 16. The accurately weighted samples ( m 0 = 0.2 g) were placed into plastic bags (with fine meshes) and the bags were immersed into 500 mL of distilled water and saline solution (0.9 wt % NaCl aqueous solution) to reach the equilibrium swelling at room temperature (25°C), respectively.…”
Section: Methodsmentioning
confidence: 99%
“…Grafting decreases from 104% for an aqueous system to 33% for 50:50 water–DMF system and continues to decrease further to 24% as the DMF content in the mixture increases to 75%. Some published work has shown that homopolymer formation takes place as a part of the graft polymerization process . Interestingly, we did not obtain any homopolymer during the grafting process suggesting that the current process leads to a better purity of the hydrogel.…”
Section: Resultsmentioning
confidence: 49%
“…Some published work has shown that homopolymer formation takes place as a part of the graft polymerization process. 33 Interestingly, we did not obtain any homopolymer during the grafting process suggesting that the current process leads to a better purity of the hydrogel. It seems that the swelling of the polymer in the grafting medium and the diffusion of monomer within the TG matrix play a significant role during the grafting.…”
Section: Resultsmentioning
confidence: 78%
“…It can be seen from the spectrum of the MPANF without hydrolysis (Fig. 2b) that the intensity of the peak at 3454 cm −1 had increased greatly, suggesting possi- [13,20,21]. The new N-H bonds may be produced during alcoholysis of nitrile groups to imidate esters.…”
Section: Ftir Spectroscope Analysismentioning
confidence: 97%