Ultra-trace determination of 226Ra in thermal waters by high sensitivity quadrupole ICP-mass spectrometry following selective extraction and concentration using radium-specific membrane disks

Joannon, Sylviane; Pin, Christian

doi:10.1039/b007682l

Cited by 41 publications

(14 citation statements)

References 24 publications

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“…For 226 Ra analysis by TIMS, Ra-Ba separations are required because the presence of Ba drastically decreases the ionization efficiency of fg Ra samples from 10% to <1%. This material has been widely used for separations of Ra from Ba (e.g., Chabaux et al 1994;Lundstrom et al 1998;Rihs et al 2000;Joannon and Pin 2001;Pietruszka et al 2002) and is a complement or alternative to cation exchange separations for EDTA complexes of these elements (Volpe et al 1991;Cohen and O'Nions 1991). Sr-Spec material would also be useful for 210 Pb analysis, since Pb has a greater distribution coefficient than Sr with this extractant.…”

Section: Extraction Chromatography Resins/disksmentioning

confidence: 98%

“…These materials were largely developed and basic separation capabilities determined at Argonne National Laboratory by P. Horwitz and colleagues and have been applied for uranium-series measurement by investigators around the world. These materials have been applied in two geometric configurations: as extraction chromatography beds for standard gravimetric column chromatography, and as disks for more rapid extraction of elements from aqueous solutions (e.g., Joannon and Pin 2001).…”

Section: Extraction Chromatography Resins/disksmentioning

confidence: 99%

See 1 more Smart Citation

Techniques for Measuring Uranium-series Nuclides: 1992-2002

Goldstein

Stirling

2003

Reviews in Mineralogy and Geochemistry

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Section: Extraction Chromatography Resins/disksmentioning

confidence: 98%

Section: Extraction Chromatography Resins/disksmentioning

confidence: 99%

Techniques for Measuring Uranium-series Nuclides: 1992-2002

Goldstein

Stirling

2003

Reviews in Mineralogy and Geochemistry

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“…However, their sample matrices – U ores for example – were particularly complex and rich in many interfering elements. Joannon and Pin (2001) present several methods, which include (a) a first elution with Dowex AG50W‐X8 and 5 mol l −1 HNO 3 followed by a second on Sr resin with 5 mol l −1 HNO 3 , a procedure directly inspired from the initial development of Chabaux et al. (1994).…”

Section: Review Of the Existing Proceduresmentioning

confidence: 99%

“…However, their sample matrices -U ores for examplewere particularly complex and rich in many interfering elements. Joannon and Pin (2001) present several methods, which include (a) a first elution with Dowex AG50W-X8 and 5 mol l -1 HNO 3 followed by a second on Sr resin with 5 mol l -1 HNO 3 , a procedure directly inspired from the initial development of Chabaux et al (1994). This procedure was also adopted by Foster et al (2004) for seawater; these authors underlined the need to re-process the Sr resin step several times, to obtain the optimum Ba-Ra separation.…”

Section: Review Of the Existing Procedures 226 Ramentioning

confidence: 99%

Single Column Sequential Extraction of Ra, Nd, Th, Pa and U from a Natural Sample

Jeandel¹,

Venchiarutti²,

Bourquin³

et al. 2011

Geostandard Geoanalytic Res

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International audienceA new procedure allowing the sequential extraction of Ra, Nd, Th, Pa and U from the same initial natural sample (sea or river waters, particles, sediments, rocks) is proposed. Extraction recoveries were better than 90%. Procedural blanks ranged from 80 pg (for Nd) to below 1 fg, the detection limit of the MC-ICP-MS used (for Pa); all were negligible compared with the amounts of elements currently determined. Based on classical anionic resins attached to a peristaltic pump allowing precise flow rate control, this procedure allowed a consequent reduction of the sample size, which improved the sampling resolution and reduced the sampling cost. It also ensured a better consistency of the samples for the five tracers

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“…The PC-Based systems are being used in "mission critical" environment and are performing as expected by the designer. The data-base for the I/O and alarms were globallydistributed to the network, requiring reduced maintenance on the system Joannon et al (2001). developed a method for the determination of 226Ra in highly saline (total dissolved solids approximately equals 6 g/L) thermal waters, using ultrasonic nebulization and a quadrupole-based instrument equipped with a high sensitivity-pumping interface.…”

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confidence: 99%

Monitoring, sampling and automated analysis

Srinivasan¹

2002

Water Environment Research

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This section presents the review i) in the area of monitoring pollutants in water/soil medium; and ii) sampling and automated analysis in water/wastewater/ groundwater treatment. Review is based on several papers published during 2001. MonitoringDel Bello et al., (2001) designed the VISIR instrument as a lightweight facility to be embarked on future low Earth orbit operational satellites whose mission requirementsinclude monitoring of open oceans, coastal zones and land surface areas. The instrument consists of an imaging spectrometer working in the visible range, a dualband thermal infrared radiometer and a single-band imager in the short-wave infrared.The instrument provides two operational modes, namely the "global mode" and the "regional mode" with steering capability. The high radiometric performances achieved in both operational modes show the capability to detect very small radiometric changes such as those induced by typical variations of the water quality parameters (chlorophyll, suspended sediments, yellow substance) and surface temperature anomalies. Gao (2001) reported that the total sediment transport under the action of flow included generally three forms of sediment transport, suspended load, density current and bed load. The author discussed about how to realize simultaneously these three forms of sediment movement in an identical physical model. Gerristen et al. (2001) discussed the modeling of suspended particulate matter (SPM) patterns and their variation on North Sea over the time scale of several months in this paper. The nature of the study was a sensitivity analysis of the various modules forming the integrated SPM model: the hydrodynamic model, the wave model and the SPM transport and erosion-sedimentation model. Whitehouse (2001) reported that the regulation of point source discharges as an important component in protecting the Literature Review 2002

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Ultra-trace determination of 226Ra in thermal waters by high sensitivity quadrupole ICP-mass spectrometry following selective extraction and concentration using radium-specific membrane disks

Cited by 41 publications

References 24 publications

Techniques for Measuring Uranium-series Nuclides: 1992-2002

Techniques for Measuring Uranium-series Nuclides: 1992-2002

Single Column Sequential Extraction of Ra, Nd, Th, Pa and U from a Natural Sample

Monitoring, sampling and automated analysis

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