“…Generally, two-dimensional (2D) nanomaterials are suitable for immobilization on the electrode surface of the electrochemical biosensor due to their unique physical and chemical features, including MoS 2 , Mo 2 C, and vanadium disulfide (VS 2 ). , VS 2 , a typical transition-metal dichalcogenides (TMDs), presents a metallic electronic ground state; hence, triple-layered stacking 2D VS 2 nanosheets exhibit superior conductivity, large specific surface area, and superior mechanical properties. − Moreover, to improve the biocompatibility, gold nanoparticles (AuNPs) are applied in biosensors due to their superior biocompatibility, large surface area, and remarkable conductivity . Therefore, VS 2 nanosheets (NS) and AuNPs could be effectively combined to immobilize more probes and accelerate electron transfer easier . Thus, the VS 2 /AuNPs nanocomposites on the modified electrode will enhance the biosensor signal greatly by increasing the charge transfer rate and efficiently retaining the biomolecule activities.…”