This study aimed to investigate the use of water hyacinth to produce liquid smoke. The study observes the temperature and time variables of yield, pH, density, and refractive index in the production of liquid smoke from water hyacinth. The sequence of the work is as follows: first, water hyacinth was cut into 5 cm sections and then sun-dried for 2–3 d, depending on the weather. Next, 550 g of dried water hyacinth was added to the pyrolysis reactor. The temperature variations were 200°C, 400°C, and 600°C, and the time variations were 1, 4, and 7 h. As a result, liquid smoke was produced with varying yield, pH, densities, and refractive indices. The best results in this research are liquid smoke pyrolysis at a temperature of 400°C and 4 h with the acquisition of a yield of 93 mL, pH 2–4, a density of 1.080,8 gr/mL, and a refractive index of 1.339,6, with chemical component 41.45% total acid, 2.44% phenol and 56.10% carbonyl.