2018
DOI: 10.1007/s11244-018-1067-2
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Various spectroelectrochemical cells for in situ observation of electrochemical processes at solid–liquid interfaces

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Cited by 13 publications
(6 citation statements)
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“…Using a thin layer cell comprising windows transparent to the incident light is mandatory, and experiments can be performed either in transmittance or fluorescence mode, although the latter is usually preferred. 67 Fig. 10 shows examples of typical XAS-SEC cells.…”
Section: Electrochemical Approachesmentioning
confidence: 99%
“…Using a thin layer cell comprising windows transparent to the incident light is mandatory, and experiments can be performed either in transmittance or fluorescence mode, although the latter is usually preferred. 67 Fig. 10 shows examples of typical XAS-SEC cells.…”
Section: Electrochemical Approachesmentioning
confidence: 99%
“…Besides, it has been reported that secondary ion yields of species on metal gold surfaces could be significantly enhanced. Furthermore, as illustrated in Figure S2 the circular edge of the perforated gold film might be pushed by the pressure inside and curved toward the vacuum direction. In such a case, a thin layer of electrolyte might form on the upper curved gold film edge, allowing the detection of secondary ion signals from the electrochemical double layer, which is similar to the principle of in situ X-ray photoelectron spectroscopy (XPS) studies of electric double layer. ,, …”
mentioning
confidence: 99%
“…In such a case, a thin layer of electrolyte might form on the upper curved gold film edge, allowing the detection of secondary ion signals from the electrochemical double layer, which is similar to the principle of in situ X-ray photoelectron spectroscopy (XPS) studies of electric double layer. 3,31,32 The real-time liquid SIMS signals in positive and negative ion modes during three consecutive CV scans were obtained and shown in Figures 2 and S3 − , which are the dominant components of anions in the electrolyte at pH of 7.0 with the molar ratio of ∼1.6 calculated according to the pK a values of H 3 PO 4 . 11 The signal trend of PO 3…”
mentioning
confidence: 99%
“…Such hardware, in principle, is already available at some APXPS setups and requires only minor customization for (micro-) PS incorporation. 1,42,43 Overall, plasma-XPS is a new emerging metrology platform that will greatly complement existing plasma chemistry studies. The main advantage of this operando method is the ability to detect short-living and/or fast-desorbing/diffusing reaction plasma-induced intermediates that are hard or impossible to interrogate using a standard before-and-after approach.…”
Section: Discussionmentioning
confidence: 99%