Nanoparticles have been widely used in the improvement of the mechanical and thermal properties of the epoxy matrix. In this study, the room temperature curing agent composed of acrylic acid and 2,4,6-trimethyl-mphenylenediamine was mixed with different concentrations of CeO 2 nanoparticles into the epoxy resin (E51) to obtain a nanocomposite that can be rapidly molded and cured. Fourier transform infrared spectroscopy and differential scanning calorimetry were used to study the curing behavior of nanocomposites and E51 with the synthesized hardener. Through tensile, flexural, and impact tests, the influence of the nanoparticles content on the mechanical and thermal properties of the prepared composites was discussed.