Vortex assisted liquid-liquid microextraction based on in situ formation of a natural deep eutectic solvent by microwave irradiation for the determination of beta-blockers in water samples

Yıldırım, Sercan; Sellitepe, Hasan Erdinç

doi:10.1016/j.chroma.2021.462007

Cited by 35 publications

(5 citation statements)

References 38 publications

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“…The resulting DES was employed for quantitative determination of metaprolol. 154 These investigations have proven the stable existence of DES formed by reacting HBA alone with the product being extracted. The resultant DES formed remains as a separate phase, which could be easily removed, achieving maximum yield of the product.…”

Section: Acs Sustainablementioning

confidence: 96%

“…Identical investigation on in situ synthesis of DES was performed by reacting thymol and azealic acid in water. The resulting DES was employed for quantitative determination of metaprolol . These investigations have proven the stable existence of DES formed by reacting HBA alone with the product being extracted.…”

Section: Sustainable Low-energy Extraction Systems With Desmentioning

confidence: 98%

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Sustainable and Green Engineering Insights on Deep Eutectic Solvents toward the Extraction of Nutraceuticals

Balaraman

Rangabhashiyam

Rangarajan

et al. 2021

ACS Sustainable Chem. Eng.

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Deep eutectic solvents (DES) hold promising potential in the selective purification of bioactive molecules from various complex sources. Although they are increasingly considered as a biocompatible extraction medium, adding the task-specific functionality, which makes DES distinctive for the selective extraction of compounds, requires appropriate tailoring of their physical properties. This critical review investigates the influential physical properties of deep eutectic solvents and their effect on various sustainable extraction methodsincluding both solid–liquid and liquid–liquidfor the separation of nutraceuticals. Various methods by which DES are employed as solvents, cosolvents, or as adjuvants in different extraction systems are compared in terms of their efficiency and selectivity. Furthermore, the correspondence between the type of DES and the nature of target nutraceuticals to be extracted is also discussed. The Review highlights the key achievements and future prospects of employing DES along with the lacunae in the current investigations and proposed various approaches for sustainable applications.

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Section: Acs Sustainablementioning

confidence: 96%

Section: Sustainable Low-energy Extraction Systems With Desmentioning

confidence: 98%

Sustainable and Green Engineering Insights on Deep Eutectic Solvents toward the Extraction of Nutraceuticals

Balaraman

Rangabhashiyam

Rangarajan

et al. 2021

ACS Sustainable Chem. Eng.

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“…The application of FrFD is that it conducts as a prelude to the optimization design, ensuring that factors being screened do indeed have a significant contribution to the responses. Many optimization designs such as CCD [19] and BBD [20] could be embedded within the subsequent optimization for further examination. For instance, Teglia et al [21] developed a gas chromatography (GC) method using an FrFD and CCD for the determination of residual solvents in pharmaceuticals.…”

Section: Factorial Designs (Fd)mentioning

confidence: 99%

Design of experiment techniques for the optimization of chromatographic analysis conditions: A review

et al. 2022

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Design of experiment (DoE) techniques have been widely used in the field of chromatographic parameters optimization as a valuable tool. A systematic literature review of the available DoE techniques applied to the development of a chromatographic analysis method is presented in this paper. First, the most common available designs and the implementation steps of DoE are comprehensively introduced. Then the studies in recent 10 years for the application of DoE techniques in various chromatographic techniques are discussed, such as capillary electrophoresis, liquid chromatography, gas chromatography, thin‐layer chromatography, and high‐speed countercurrent chromatography. Current problems and future outlooks are finally given to provide a certain inspiration of research in the application of DoE techniques to the different chromatographic techniques field. This review contributes to a better understanding of the DoE techniques for the efficient optimization of chromatographic analysis conditions, especially for the analysis of complex systems, such as multicomponent drugs and natural products.

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“…9 They compared the results from high-performance liquid chromatography (HPLC) and gas chromatography (GC) combined with various detectors. 9 Sample types to which HPLC-based methods have been applied to quantify β-blockers include water 10,11 and pharmaceutical preparations, 12,13 and also biological samples such as urine, 14,15 plasma 15,16 and blood. 17 The most suitable alternative to HPLC might be capillary electrophoresis (CE), featuring versatility, high separation efficiency, short analysis times, and reduced sample and reagent consumption.…”

Section: Introductionmentioning

confidence: 99%

Electrochemical screening of selected β-blockers at a polarized liquid–liquid interface

Sobczak,

Rudnicki,

Poltorak

2024

Analyst

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Vortex assisted liquid-liquid microextraction based on in situ formation of a natural deep eutectic solvent by microwave irradiation for the determination of beta-blockers in water samples

Cited by 35 publications

References 38 publications

Sustainable and Green Engineering Insights on Deep Eutectic Solvents toward the Extraction of Nutraceuticals

Sustainable and Green Engineering Insights on Deep Eutectic Solvents toward the Extraction of Nutraceuticals

Design of experiment techniques for the optimization of chromatographic analysis conditions: A review

Electrochemical screening of selected β-blockers at a polarized liquid–liquid interface

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