“…The corresponding XPS peaks of Fe, Co, N, O, and C in FeCoÀ NC-9.5 can be observed in Figure S2, indicating the existence of Fe, Co, O, and N in the catalyst. The C 1s spectrum of Fe 1 Co 1 À NC-9.5 is deconvoluted into four peaks at about 289.8, 287.4, 285.5, and 284.7 eV (Figure 2a), which can be assigned to CÀ C, CÀ N, CÀ O, and C=O bonds, respectively [35]. The presence of the CÀ N bond confirms that NC has been successfully obtained, which is conducive to the introduction of defects and thus the highly exposed active sites.…”