Ninety-nine blood samples were collected in Egypt during 2003-2004 (85 males' and 14 female's) aged between twenty five and sixty years old from both diagnosed liver and bladder cancer patients in addition to high-risk people to these types of cancers such as hepatitis C virus and chronic bilharzias as well as apparently healthy people as a control. The collected blood samples passed through separation of serum, extraction, evaporation, concentration and determination using gas liquid chromatography equipped with electron capture detector. The monitoring of 14 organochlorine pesticides, characterized by their long persistence in human tissues which are HCB, alpha-HCH, beta-HCH, gamma-HCH, delta-HCH, Aldrin, Dieldrin,
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