This research aims to study the growth and the effect of annealing temperature on the structural properties of Platinum/YSZ/Platinum thin film. The thin films were prepared by RF and DC magnetron sputtering method utilized platinum as electrodes (anode and cathode) and YSZ as electrolyte. Two temperatures of annealing (400 and 600 °C) were conducted onto Platinum/YSZ/Platinum thin film for comparison in this study. Crystalline phase, microstructure and thickness of thin films were evaluated using X-Ray Diffraction (XRD) and Field Emission Scanning Electron Microscope (FE-SEM) technique. Results show that Pt/YSZ/Pt thin film without post-annealing gives a better morphology and crystal phase.
In this research, the effect of PEG 2000 and Degussa P25 as additives on the characteristic of Ag-TiO2 coating was reported. The TiO2 coatings were produced via sol gel method using titanium (IV) isopropoxide (TTiP) as a precursor from solutions that contains additive and without additive. Seven layers of TiO2 coating were deposited on specially made unglazed ceramic tiles produced from waste glass. All coatings were deposited using dip coating technique and were sintered at 500 °C. The TiO2 coating was then immersed in an Ag nanoparticles solution before dried at 90 °C in an oven to form Ag-TiO2 coating. The coating phases and coating morphologies were analyzed using GAXRD and SEM analysis, respectively. Results show that Ag-TiO2 coating added with Degussa P25 additive exhibits a presence of more anatase and more homogenous microstructure which gives advantages for antimicrobial application as compared to others
Sol-gel dip-coating technique was utilized to prepare Ag-TiO2 coating with additive (Degussa P25) on unglazed ceramic tiles. Three different numbers of coating layers (5, 7 and 10 layers) were deposited on unglazed ceramic tiles made of waste glass. The coatings were sintered at 500 °C with the heating rate of 2 °C/min. The crystalline phase and cross sectional areas of the coatings were evaluated using GAXRD and SEM analysis, respectively. Results showed that the average thickness of the coating increased from 7 µm to 9 µm and to 12 µm for 5, 7 and 10 coating layers, correspondingly. Coating of 10 layers exhibited a high crystallinity of anatase phase, a good surface morphology without significant cracks, and a homogeneous coating compared to the 5 and 7 layers of coating, which suggested a better performance in Ag-TiO2 coating.
This research aims to determine the effect of silver nanoparticles concentrations as antimicrobial coatings when doped to TiO2 coatings. The TiO2 coatings were prepared by sol–gel method initiating Titanium Isopropoxide–Propanol mixture as a precursor solution. The silver nanoparticles (40 nm) were then doped to the coating after sintering at 500°C. Two concentrations of silver nanoparticles, (50 ppm and 1000 ppm), were prepared for comparison in this study. Microstructure and crystalline phase of coatings were evaluated using Scanning Electron Microscope (SEM) and Glancing Angle X-Ray Difraction (GAXRD) technique. The antibacterial test was according to McFarland standard for detecting E.Coli, S.Aerues, fungas and Methicillin-Resistant Staphylococcus Aureus (MRSA). Results show that only coatings with the concentrations of 1000 ppm of silver nanoparticle function as antimicrobial coatings.
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