We demonstrate that commercially available poly(D,L-lactic acid) (PDLLA) is a suitable material for the fabrication of biodegradable optical fibers with a standard heat drawing process. To do so we report on the chemical and optical characterization of the material. We address the influence of the polymer processing on the molecular weight and thermal properties of the polymer following the preparation of the polymer preforms and the fiber optic drawing process. We show that cutback measurements of the first optical fibers drawn from PDLLA return an attenuation coefficient as low as 0.11 dB/cm at 772 nm, which is the lowest loss reported this far for optical fibers drawn from bio-resorbable material. We also report on the dispersion characteristics of PDLLA, and we find that the thermo-optic coefficient is in the range of −10 −4°C−1. Finally, we studied the degradation of PDLLA fibers in vitro, revealing that fibers with the largest diameter of 600 µm degrade faster than those with smaller diameters of 300 and 200 µm and feature more than 84% molecular weight loss over a period of 3 months. The evolution of the optical loss of the fibers as a function of time during immersion in phosphate-buffered saline indicates that these devices are potential candidates for use in photodynamic therapy-like application scenarios.

Abstract.A broad review is given of microstructured fiber optics components -light guides, image guides, multicapillary arrays, and photonic crystal fibers -fabricated using the stack-and-draw method from various in-house synthesized oxide soft glasses at the Glass Department of the Institute of Electronic Materials Technology (ITME). The discussion covers fundamental aspects of stack-and-draw technology used at ITME, through design methods, soft glass material issues and parameters, to demonstration of representative examples of fabricated structures and an experimental characterization of their optical properties and results obtained in typical applications. Specifically, demonstrators include microstructured image guides providing resolution of up to 16000 pixels sized up to 20 µm in diameter, and various photonic crystal fibers (PCFs): index-guiding regular lattice air-hole PCFs, hollow core photonic bandgap PCFs, or specialty PCFs like highly birefringent microstructured fibers or highly nonlinear fibers for supercontinuum generation. The presented content is put into context of previous work in the area reported by the group of authors, as well as other research teams.

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