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In this study, a sliding mode surface controller (SMC) designed for a quadcopter is experimentally tested. The SMC was combined with disturbance observers in six degrees of freedom of the quadcopter to effectively reject external disturbances. While respecting stability conditions all control parameters were automatically initialized and tuned using a simulation-based offline particle swarm optimization (PSO) algorithm, followed by onboard manual fine-tuning. To demonstrate its superiority, the SMC was compared with a PSO-optimized PID controller in terms of agility, stability, and the accurate tracking of hover, rectangular, and figure-eight pattern trajectories. To evaluate its robustness, the SMC controller was extensively tested in a small, enclosed, turbulent space while being subjected to a series of external disturbances, such as hanging payloads and lateral wind.