Faults involving phyllosilicates appear weak when compared to the laboratory‐derived strength of most crustal rocks. Among phyllosilicates, talc, with very low friction, is one of the weakest minerals involved in various tectonic settings. As the presence of talc has been recently documented in carbonate faults, we performed laboratory friction experiments to better constrain how various amounts of talc could alter these fault's frictional properties. We used a biaxial apparatus to systematically shear different mixtures of talc and calcite as powdered gouge at room temperature, normal stresses up to 50 MPa and under different pore fluid saturated conditions, i.e., CaCO3‐equilibrated water and silicone oil. We performed slide‐hold‐slide tests, 1–3000 s, to measure the amount of frictional healing and velocity‐stepping tests, 0.1–1000 µm/s, to evaluate frictional stability. We then analyzed microstructures developed during our experiments. Our results show that with the addition of 20% talc the calcite gouge undergoes a 70% reduction in steady state frictional strength, a complete reduction of frictional healing and a transition from velocity‐weakening to velocity‐strengthening behavior. Microstructural analysis shows that with increasing talc content, deformation mechanisms evolve from distributed cataclastic flow of the granular calcite to localized sliding along talc‐rich shear planes, resulting in a fully interconnected network of talc lamellae from 20% talc onward. Our observations indicate that in faults where talc and calcite are present, a low concentration of talc is enough to strongly modify the gouge's frictional properties and specifically to weaken the fault, reduce its ability to sustain future stress drops, and stabilize slip.
High-pressure fluid injection in deep georeservoirs can induce earthquakes. Recent observations suggest that cyclic injections might trigger less seismicity than monotonic injections. Here, we report triaxial laboratory experiments conducted on faulted quartz-rich sandstone that provide new insight into the physics of fault-fluid interactions subjected to cyclic fluid pressure variations. The experiments were performed at 30 and 45 MPa confining pressure, imposing constant or sinusoidal fluid pressure oscillations of amplitudes ranging from 0 to 8 MPa in addition to a far-field constant loading rate (10 −4 and 10 −3 mm s −1 ). The results show that (i) in agreement with the Mohr-Coulomb theory, faults reactivate at the static friction criterion, which is generally reached at the maximum fluid pressure during oscillations. (ii) Oscillating fluid pressure perturbations promote seismic behavior rather than aseismic slip, and (iii) increasing the oscillation's amplitude enhances the onset of seismic activity along the fault. We demonstrate that this behavior is caused by slip rate variations resulting from the fluid pressure oscillations. Without fluid pressure oscillations, increasing the far-field loading rate also promotes seismic activity. Our experiments demonstrate that the seismicity intensification due to cyclic fluid injections could be promoted at shallow depth, where confining pressure is relatively low, resulting in large strain rate perturbations.
Abstract. Graphitization, or the progressive maturation of carbonaceous material, is considered an irreversible process. Thus, the degree of graphite crystallinity, or its structural order, has been calibrated as an indicator of the peak metamorphic temperatures experienced by the host rocks. However, discrepancies between temperatures indicated by graphite crystallinity versus other thermometers have been documented in deformed rocks. To examine the possibility of mechanical modifications of graphite structure and the potential impacts on graphite thermometry, we performed laboratory deformation experiments. We sheared highly crystalline graphite powder at normal stresses of 5 and 25 megapascal (MPa) and aseismic velocities of 1, 10 and 100 µm s−1. The degree of structural order both in the starting and resulting materials was analyzed by Raman microspectroscopy. Our results demonstrate structural disorder of graphite, manifested as changes in the Raman spectra. Microstructural observations show that brittle processes caused the documented mechanical modifications of the aggregate graphite crystallinity. We conclude that the calibrated graphite thermometer is ambiguous in active tectonic settings.
The underground disposal of high‐level nuclear waste is a pressing issue for several countries. In Switzerland, the Opalinus Clay formation is a shale with favorable barrier properties. However, small‐to‐large faults intersecting the formation bring the long‐term integrity of the future repositories into question. Here we present the first systematic laboratory study on the frictional strength, stability, dilatancy, and permeability of simulated Opalinus Clay gouge under typical repository conditions. Wet gouges exhibit an extremely low coefficient of friction (μf~0.16), velocity‐strengthening behavior, and shear‐enhanced dilatancy at the onset of slip, and permeability increase. Conversely, dry gouges remain weak (μf~0.36) but exhibit a transition from unstable to stable sliding with increasing sliding velocity. Thus, we infer that faults hosted in Opalinus Clay could be easily reactivated via aseismic creep, possibly acting as poor fluid conduits. However, if temporarily dried, the faults become potentially unstable, at least, at low sliding velocities (<~10 μm/s).
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