Non Interaction Approximation (NIA) is currently used to relate effective elastic moduli to crack density. It also allows one to identify the anisotropy of the crack network. We investigated thermally cracked glass sample and quantified the crack network (using SEM). From elastic wave velocity measurements, using EMT, we obtained the crack densities: 1 =0.038 (horizontal one) and 3 =0.0037 (vertical one). From SEM observations and image processing we could identify all cracks, count them and determine independently the crack density. These results agree with the previously determined ones from the elastic wave velocity measurements (within a small uncertainty range). These results indicate that the NIA is quite accurate in the considered range of crack densities, and elastic wave velocity measurements can provide reliable information on their crack distribution and crack density.
A crack network is introduced in glass by quenching heated samples. The sharp variation of temperature at the sample boundaries leads to tensile stresses that nucleate cracks. Then, they propagate in the entire sample. Quenching has been performed at 100, 200 and 300 • C. Cracks have been imaged with a scanning electron microscope. A transverse isotropic crack network is observed. Crack length and orientation have been measured. Obtained crack density has been compared to that inferred from elastic wave velocity measurements using effective medium theory. Cracked samples have been then submitted to creep tests. Two samples have been recovered, one before its failure and another after. Our observations show that vertical crack propagation takes place during brittle creep and that tertiary creep leads to a localized failure in a shear plane. The damaged and post-mortem microstructural networks have been documented.
An experimental work is presented that aimed at improving our understanding of the mechanical evolution of cracks under brittle creep conditions. Brittle creep may be an important slow deformation process in the Earth's crust. Synthetic glass samples have been used to observe and document brittle creep due to slow crack‐propagation. A crack density of 0.05 was introduced in intact synthetic glass samples by thermal shock. Creep tests were performed at constant confining pressure (15 MPa) for water saturated conditions. Data were obtained by maintaining the differential‐stress constant in steps of 24 h duration. A set of sensors allowed us to record strains and acoustic emissions during creep. The effect of temperature on creep was investigated from ambient temperature to 70°C. The activation energy for crack growth was found to be 32 kJ/mol. In secondary creep, a large dilatancy was observed that did not occur in constant strain rate tests. This is correlated to acoustic emission activity associated with crack growth. As a consequence, slow crack growth has been evidenced in glass. Beyond secondary creep, failure in tertiary creep was found to be a progressive process. The data are interpreted through a previously developed micromechanical damage model that describes crack propagation. This model allows one to predict the secondary brittle creep phase and also to give an analytical expression for the time to rupture. Comparison between glass and crystalline rock indicates that the brittle creep behavior is probably controlled by the same process even if stress sensitivity for glass is lower than for rocks.
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