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The design and construction of a promising electrode is attractive for the sensitive and selective detection of hydrazine. Here, hollow CoS2/N-doped mesoporous graphite carbon nanocages (CoS2/HNGC) were synthesized derived from ZIF-8@ZIF-67 by annealing and sulfidation. In situ nitrogen coordination and self-compounding porous carbon with hollow structure can effectively improve electrocatalytic performance and electron transfer rate of catalyst electrode. The sensor has good performance for hydrazine with a wide linear range of 1 μM - 3 mM, high sensitivity of 2384 μA mM-1 cm-2, and detection limit of 0.272 μM (S/N = 3). In addition, the fine selectivity and the application of this sensor in food hydrazine detection suggest that CoS2/HNGC can be used as an efficient electrochemical detection material for hydrazine.

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