Adhesives are increasingly being employed in industrial applications as a replacement for traditional mechanical joining methods, since they enable improvements in the strength-to-weight ratio and lower the cost of the overall structures. This has led to a need for adhesive mechanical characterisation techniques that can provide the data needed to build advanced numerical models, allowing structural designers to expedite the adhesive selection process and grant precise optimisation of bonded connection performance. However, mechanically mapping the behaviour of an adhesive involves numerous different standards resulting in a complex network of various specimens, testing procedures and data reduction methods that concern techniques which are exceedingly complex, time-consuming, and expensive. As such, and to address this problem, a novel fully integrated experimental characterisation tool is being developed to significantly reduce all the issues associated with adhesive characterisation. In this work, a numerical optimisation of the unified specimen’s fracture toughness components, comprising the combined mode I (modified double cantilever beam) and II (end-loaded split) test, was performed. This was achieved by computing the desired behaviour as a function of the apparatus’ and specimens’ geometries, through several dimensional parameters, and by testing different adhesives, widening the range of applications of this tool. In the end, a custom data reduction scheme was deduced and set of design guidelines was defined.

Adhesives are more relevant in the industrial world each day, and the need for fast, simple, and cheap mechanical characterization techniques is urgent. During the following work, a novel specimen that can perform four different tests in only one go, is used to numerically study the effect of downgrading the properties of the substrate materials allowing higher sensitivity when characterizing non-structural adhesives. This study showed that numerically the load displacement curves of fracture tests are the most influenced ones, but the actual change in the fracture toughness from steel to aluminum substrates is negligible for the mode I loading and penalizing for the mode II loading.

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Adhesives are extensively used in the automotive and aeronautical industries as they enable the creation of durable and light weight joints, with exceptional strength to weight ratios. The constant search for the means of adapting the mechanical performance of adhesives to each application has led to the use of several types of fillers to change their properties. Following a study on the effect of inorganic fillers, i.e., hollow glass beads, in the failure mechanisms of single lap joint’s (SLJ), this work focuses on the response of the strength and fracture properties of structural adhesives to this filler. To this end, their tensile strength and mode I fracture properties were thoroughly analyzed by performing bulk tensile and double-cantilever beam (DCB) tests, at a quasi-static speed. The specimens were manufactured by adding different %v/v of filler to two epoxy-based crash resistant adhesives. Both adhesives have shown a negligible effect on the tensile strength, a decrease in strain at failure and critical energy release rate in mode I, as well as an increase of the Young’s modulus, for higher % in volume of hollow glass beads. These phenomena were further analyzed recurring to scanning electron microscopy, and the concept of rule of mixtures.