In this study, the extraction efficiency of natural deep eutectic solvents (NADES) based on choline chloride as a hydrogen bond acceptor (HBA) and five different hydrogen bond donors (HBD; lactic acid, 1,4-butanediol, 1,2-propanediol, fructose and urea) was evaluated for the first time for the isolation of valuable bioactive compounds from Achillea millefolium L. The phytochemical profiles of NADES extracts obtained after ultrasound-assisted extraction were evaluated both spectrophotometrically (total phenolic content (TPC) and antioxidant assays) and chromatographically (UHPLC-MS and HPLC-UV). The results were compared with those obtained with 80% ethanol, 80% methanol, and water. The highest TPC value was found in the lactic acid-based NADES (ChCl-LA), which correlated with the highest antioxidant activity determined by the FRAP analysis. On the other hand, the highest antiradical potential against ABTS+• was determined for urea-based NADES. Phenolic acids (chlorogenic acid and dicaffeoylquinic acid isomers), flavones (luteolin and apigenin), and their corresponding glucosides were determined as the dominant individual phenolic compounds in all extracts. The antibacterial and antifungal properties of the extracts obtained against four bacterial cultures and two yeasts were evaluated using two methods: the agar dilution method to obtain the minimum inhibitory concentration (MIC) and the minimum bactericidal or fungicidal concentration (MBC or MFC), and the disc diffusion method. ChCl-LA had the lowest MIC and MBC/MFC with respect to all microorganisms, with an MIC ranging from 0.05 mg mL−1 to 0.8 mg mL−1, while the water extract had the weakest inhibitory activity with MIC and MBC/MFC higher than 3.2 mg mL−1.
The paper explores the relationship between subjective assessment of wearing comfort and objectively determined physiological parameters (mean skin temperature, skin relative humidity, amount excreted in sweat absorbed in clothing) in a warm environment. The experiment involved five young girls who wore two different models of women’s summer clothing (women’s dresses and women’s blouse plus shorts) made from five different raw materials, but of nearly identical structural characteristics . The investigation consisted of 450 individual tests. All wearing trial tests were performed under artificially designed ambient conditions within a computer-controlled climatic chamber. It was found that there existed a relationship between subjective assessment of wearing comfort and objectively determined physiological parameters of the test subjects. The statistical analysis results showed that coefficients of multiple linear regression in dependence of the subjective assessment of the degree of skin moisture Wskin on climatic conditions had the value of R2 = 0.87, based on physiological parameters, such as skin temperature Tskin and skin relative humidity RHskin (R2 = 0.90), and on the amount of excreted sweat Esweat and the amount of sweat absorbed within clothing Wsweat (R2 = 0.87).
The middle of the last century presents the beginning of a wide use of heat technologies for joining of the textile materials. Up to now, adhesive bonding/fusing of textile materials by application of heat and pressure during the determinate time has become a wide-use technology for manufacturing numerous kinds of textile products, such as outdoor and sport garments, underwear, swimming suits, medical gowns, toys, and automotive seating fabrics. Fusing and welding technologies of textiles represent today a significant competition to traditional sewing, because the technological process is quick and energy efficient. The welding and fusing of textiles represent a great opportunity for providing a good performance as well as aesthetic appearance. New types of fusing/ welding machines with high technological solutions regarding the functions, low energy consumptions, and environmental-friendly effects are placed on the market. This chapter presents fusing, hot air and hot wedge welding techniques, suitable for joining of textile materials. The theoretical background and fundamental working principles of the equipment for each technology are presented in the first part of the chapter. Special attention is given to presentation of thermoplastic adhesives, textile substrates for fusible interlinings, and welding tapes. Next, the fusing/welding methods and their parameters are described, and the methods for quality evaluation of fused/welded panels are presented. The effect of fusing/welding parameters, selected methods depending on applied fabrics, fusible interlinings and welding tapes, and used fusing/welding machines are discussed separately. Factors effecting the quality of fused and hot air/ wedge welded panels are supported with latest scientific findings. The advantages and disadvantages of the presented techniques are discussed together with the applications areas of each of the presented techniques. The new application opportunities are also highlighted at the end of the chapter.
The surface of textile materials is highly textured, commonly in non-uniform ways. Because of this texture effect, textile surface appears rougher and more porous than other printing substrates, which can cause excessive ink penetration during printing process. Next, washing process is very important factor because it influences ink characteristics on printed samples as well as structural changes of the textile substrate. The aim of this paper is to determine the influences of washing process and different mesh tread count used for printing on print quality. This will be obtained by using spectrophotometric analysis, and GLCM image processing method for print mottle estimation. The results of this research show that increasing number of washing processes leads to higher color differences reproduction color in comparison to printed materials before washing. It also shows that textile surface texture has a great influence on print mottle as well as that number of washing treatment series can generate variations of solid-tone print uniformity.
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