A Cu–1.1%Cr–0.04%Zr (wt.%) alloy was processed by severe plastic deformation (SPD) using the equal channel angular pressing (ECAP) technique at room temperature (RT). It was found that when the number of passes increased from one to four, the dislocation density significantly increased by 35% while the crystallite size decreased by 32%. Subsequent rolling at RT did not influence considerably the crystallite size and dislocation density. At the same time, cryorolling at liquid nitrogen temperature yielded a much higher dislocation density. All the samples contained Cr particles with an average size of 1 µm. Both the size and fraction of the Cr particles did not change during the increase in ECAP passes and the application of rolling after ECAP. The hardness of the severely deformed Cu alloy samples can be well correlated to the dislocation density using the Taylor equation. Heat treatment at 430 °C for 30 min in air caused a significant reduction in the dislocation density for all the deformed samples, while the hardness considerably increased. This apparent contradiction can be explained by the solute oxygen hardening, but the annihilation of mobile dislocations during annealing may also contribute to hardening.

<p class="AMSmaintitle"><span lang="EN-US">Ultrafine grained materials are capable of superplastic elongation at strain rates faster than those currently employed for commercial superplastic forming operations. However, such operations require the material in the form of thin sheets. Asymmetric rolling (ASR), as one of severe plastic deformation (SPD) methods, was used to make ultra-fined grain materials with enhanced performance. This work show effect of the deformation paths on micro-hardness and mechanical properties changing during asymmetric rolling of pure aluminium. In our case, the asymmetric condition was introduced by using different diameters with a ratio of upper and bottom roll 2,4. The thickness of samples was reduced about 20% - 40% at ambient temperature and at cryogenic temperature. Asymmetric rolling at cryogenic temperature (ASR-C) provides greater strength tensile properties than rolling at ambient temperature (ASR-A). </span></p>

This work deals with comparing the mechanical properties of OFHC copper and CuCrZr alloys processed by asymmetric ambient rolling (ASaR) and asymmetric cryorolling (AScR). The conditions for asymmetrical rolling were ensured by different diameters of the main rolls. The thickness of samples was reduced about 20% - 70% at ambient temperature and at a temperature of liquid nitrogen. Mechanical properties such as yield strength, tensile strength, reduction of area and microhardness were determined for all rolled samples. Rolling at cryogenic temperatures provide about 50-60MPa more tensile strength for Cu and 60-80 MPa for CuCrZr alloys when rolling at ambient temperature. After AScR of CuCrZr alloys, a start of precipitation was shifted at the temperature of 434∘C and recrystallization was a part of the precipitation peak. According to the results, plastic deformation through shear bands is the dominant mechanism in materials with lower stacking fault energy (CuCrZr) treated under cryogenic conditions.

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