In this research, the effects of hybrid nanoparticles Fe3O4+Ni on the magnetic and dielectric properties of epoxy resin are investigated. Microstructural characterization was performed by Field Emission scanning electron microscopy FESEM, X-ray diffraction spectra XRD, and Fourier-transform infrared spectroscopy (FTIR). The magnetic properties were investigated by vibrating sample magnetometer (VSM) and the dielectric response was investigated by a precision impedance analyzer (Agilent 4294A) LCR meter at room temperature with different frequencies. The study dealing with hybrid nanocomposite (epoxy/Fe3O4+Ni) consisting of epoxy resin as the matrix material reinforcing by magnetite nanoparticles (Fe3O4) with different weight percentages (3wt.%, 6wt.%, 9wt.%, 12wt.%, 15wt. %) and constant weight percentage 2wt% of nickel (Ni) nanoparticles. The samples were prepared using the casting method. The epoxy with the hardener is weighted and mixing in a 2:1 ratio and then add reinforcement materials Fe3O4+Ni into the epoxy. Microstructural analysis showed that a uniform distribution and homogeneously dispersed in the epoxy matrix. The results of this work exhibit that the Increasing additive weight percentages of Fe3O4 nanoparticles with a constant weight of Ni nanoparticles into epoxy resin led to improvement in the magnetic and electric properties of hybrid nanocomposites compared with pure epoxy.
In this paper, study the effects of magnetite nanomaterial Fe3O4 on the mechanical properties of epoxy. Dispersion of Fe3O4 nanoparticles in the epoxy resin was performed by ultrasonication. The samples of the nanocomposites were prepared using the casting method. The nanocomposites contain epoxy resins as a matrix material incorporated by different weight percentages of magnetite Fe3O4 that varies from 0wt.% to 15wt.% as a reinforcing material. The epoxy with the additive reinforcement materials Fe3O4 was slowly mixed in a sonication bath for 15 minutes, then the mixture poured into silicon molds. Field Emission Scanning Electron Microscopy FESEM and X-ray diffraction spectra XRD were used to characterize the morphological and structural properties of preparing samples and the distribution of Fe3O4 nanoparticles to the epoxy resin. Mechanical testing consists of tensile, hardness shore, and three-point flexural tests were performed on the samples at room temperature according to ASTM standards. The results showed that reinforcement by 15wt.% of Fe3O4 nanoparticles maximizes these mechanical properties of nanocomposites compared with pure epoxy except for the young modulus's preferred weight at 9 wt.%, this is due to aggregation of the additives nanomaterials in epoxy resin above 9 wt.%.
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