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In this study, flower-like MoS2 nanomaterials were synthesized by hydrothermal method with excess thiourea. The adsorption performance of MoS2 adsorbent for methylene blue (MB) in azo dye wastewater was studied. The morphology, crystal phase, and microstructure of nano MoS2 samples were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectroscopy, and Fourier transform infrared spectroscopy. The effects of adsorption isotherm, kinetics, different hydrothermal time, and pH on the adsorption experiment were studied. The results showed that the MoS2 adsorbent with a hydrothermal time of 1 h had good adsorption properties for MB. The adsorption data accord with the Langmuir isotherm model, and the maximum adsorption capacity of MoS2 adsorbent is 200 mg/g, and the adsorption kinetics agrees well with the pseudo two-level model. The removal rate of MB is not significantly affected by the pH values. The large pH range can still maintain the removal rate above 93.47%, and the regeneration and recovery properties of MoS2 were also explored. Finally, the adsorption mechanism of MoS2 on MB is discussed.

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