This study investigates the influence of surface treatment of contaminated lithium disilicate and leucite glass ceramic restorations on the bonding efficacy of universal adhesives. Lithium disilicate and leucite glass ceramics were contaminated with saliva, and then cleaned using distilled water (SC), or 37% phosphoric acid (TE), or hydrofluoric acid (CE). Specimens without contamination served as controls. The surface free energy was determined by measuring the contact angles formed when the three test liquids were placed on the specimens. Bond strengths of the universal adhesives were also measured. Saliva contamination and surface treatment of ceramic surfaces significantly influenced the surface free energy. The bond strengths of universal adhesives were also affected by surface treatment and the choice of adhesive materials. Our data suggest that saliva contamination of lithum disilicate and leucite glass ceramics significantly impaired the bonding of the universal adhesives, and reduced the surface free energy of the ceramics.

This study evaluated the effect of a calcium phosphate desensitizer on the demineralization of bovine dentin by measuring changes in transmitted ultrasonic velocity. Bovine dentin specimens with and without application of desensitizer were immersed in 0.1 M lactic-acid buffer solution (pH 4.75) 10 min twice daily throughout the test period, and stored in artificial saliva solution (pH 7.0) between treatments. The propagation time of longitudinal ultrasonic waves was measured by a pulser-receiver. Data were evaluated using one-way ANOVA followed by Tukey HSD test (α=0.05). The ultrasonic velocity decreased over time in specimens stored in demineralizing solution (3,785-3,462 m/s); however, desensitizer-applied specimens had a significantly higher sonic velocity (3,945-3,990 m/s) than those without application. The calcium phosphate desensitizer appeared to reduce the demineralization of dentin and occluded dentinal tubules.