A superior lamellae etching drop-off technique is described for the preparation of W tips without the use of CCl4. Sharp tips with an apex of 25 nm or less can be produced routinely. In the case of Pt/Ir wire, the chemical inertness of the material means that it has to be reduced in diameter before being etched to yield a tip. In order to accomplish this, a capillary diameter reduction technique has also been developed for use in combination with the lamellae etching drop-off technique. The apparatus does not require the use of micromanipulators or micromovers. The shapes of tips with apexes as small as 25 nm can be investigated by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). This low cost method of producing sharp tips scanning tunneling microscopy is very effective and it would probably be feasible to develop an automatic tip preparation with a little more technical effort. Since it is possible to produce well shaped W tips almost every time after acquiring a little skill, it is not usually necessary to check their shape by TEM or SEM before use. In contrast, the success rate with Pt/Ir tips is only up to 70%, so that it is advisable to check their shapes by TEM.

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The network analysis method was applied to AT cut quartz blanks (f(0) = 10 MHz), which were loaded with liquids of low and medium viscosity (water, methanol, ethanol, 1-propanol, 1-butanol, glycerol solutions). The shift of the resonance frequency Δf could be separated into a term due to rigidly coupled mass Δf(rig) and a term due to viscous damping Δf - Δf(rig). From the difference Δf - Δf(rig) and the broadening of the resonance curve, the complex shear modulus G = G' + iωη(L) was calculated. The viscosity coefficients η(L) are in good agreement with literature data. As G' > 0, it can be concluded that the examined fluids also reveal elasticity at shear frequencies in the MHz range. For the low-viscosity liquids, elastic contributions resulting from collective interactions of molecules are measurable but small and neglectable in most applications. The medium viscous liquid glycerol (98%) begins to exhibit considerable elasticity, resulting from the relaxation of separate molecules.