The present work was targeted to design a surface against cell seeding and adhering of bacteria, Bacillus subtilis. A multi-walled carbon nanotube/titanium dioxide nano-power was produced via simple mixing of carbon nanotube and titanium dioxide nanoparticles during the sol-gel process followed by heat treatment. Successfully, quercetin was immobilized on the nanocomposite via physical adsorption to form a quercetin/multi-walled carbon nanotube/titanium dioxide nanocomposite. The adhesion of bacteria on the coated-slides was verified after 24 h using confocal laser-scanning microscopy. Results indicated that the quercetin/multi-walled carbon nanotube/titanium dioxide nanocomposite had more negativity and higher recovery by glass surfaces than its counterpart. Moreover, coating surfaces with the quercetin-modified nanocomposite lowered both hydrophilicity and surface-attached bacteria compared to surfaces coated with the multi-walled carbon nanotubes/titanium dioxide nanocomposite.
Carboxymethyl β-cyclodextrin–nanochitosan–glutaraldehyde (CM-βCD:nChi:Glu) terpolymer was prepared as a nano-adsorbent for the removal of the anionic textile dye, acid red 37. The terpolymer nanocomposite formation and characterization were clarified by FTIR, XRD, scanning electron microscopy, TEM, Brunauer–Emmett–Teller specific surface area (BET-SSA), and zeta potential. The removal of the textile dye was investigated by using the batch adsorption method, investigating the effect of pH, dye concentration, adsorbent dose, contact time, and temperature. The results revealed that the maximum removal efficiency of 102.2 mg/L of the dye is about 99.67% under pH 6.0, the optimal contact time is 5 min, and the adsorbent dosage is 0.5 g/L. At 29°C; the adsorption capacity increased from 81.29 to 332.60 mg/g when the initial concentration of the dye was increased from 40.97 to 212.20 mg/L. Adsorption kinetics fitted well with the pseudo–second-order model with a good correlation (R2 = 0.9998). The Langmuir isotherm model can best describe the adsorption isotherm model. Based on the experimental results, the CM-βCD:nChi:Glu terpolymer has a promising potential as an efficient novel adsorbent for the removal of textile dye acid red 37 from contaminated water. This study’s preparation techniques and demonstrated mechanisms offer valuable insights into the adsorbent–adsorbate interactions mechanism, analysis, challenges, and future directions of beta-cyclodextrin/chitosan–based adsorbents in wastewater treatment.
In this paper, we report the synthesis of Fe3O4 nanoparticles which are resistant to surface poisoning, has been adopted. Fe3O4 nanoparticles have been successfully coated with Au in the form of a shell with different sizes (Fe3O4/Au Core/Shell). Adjustment of the components’ ratio makes the shell thickness of the core/shell particles tunable. Thus, the presented route yields well-defined core/shell structures of different sizes in the range 15–57[Formula: see text]nm with varying the proportion of Au noble metal to Fe3O4 nanoparticles. The UV-Visible absorption spectra, X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM) were applied for the characterization of the formed core/shell structures. Moreover, magnetic properties of the core/shell nanocomposites were also studied using Vibrating Sample Magnetometry (VSM).
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