Cemented optical components and groups are essential devices for the realisation of modern systems and apparatuses used in a broad range of different applications such as telecommunications, imaging and even surgery. However, various parameters may affect the stability of cemented connections. In this context, the impact of dielectric barrier discharge plasma at atmospheric pressure on the adhesiveness of cemented glass components was evaluated in the present work. For this purpose, the plasma-induced change in surface wettability and energy as well as the cement’s adhesive pull strength was measured. Investigations were performed on samples, which were subject to different procedures of artificial ageing. It is shown that the adhesive pull strength of cemented glass components was notably increased after a short-term plasma treatment of merely 10 s due to an enhanced wettability of the applied UV-curing optical cement. The pull strength, i.e., the adhesiveness of cemented glasses was increased by a factor of 2.1 to 4.6, depending on the particularly applied artificial ageing procedure. The results and findings finally demonstrate the high potential of the applied short-term plasma treatment as a cleaning and surface activation step in optics manufacturing on an industrial scale.
In this contribution, we present a plasma-based approach for modifying the focal length of plano-convex lenses realised by the deposition of droplets made of optical cement. For this purpose, PMMA and soda-lime glass substrates were treated with a direct dielectric barrier discharge plasma at low pressure. To obtain plasma-induced changes in surface energy of the substrates by the formation of functional groups, octafluorocyclobutane (C4F8) was used as process gas. Such treatment lead to a notable decrease in surface energy and especially its polar fraction, which is attributed to the generation of fluorocarbon compounds such as polytetrafluoroethylene (PTFE) as also confirmed by FTIR spectroscopic measurements. It is shown that this effect has a considerable impact on the contact angle and radius of curvature, respectively, of the deposited cement droplets where differences by a factor of about two were obtained. After curing of the cement, front focal lengths in the range from approx. 5 to 13 mm were realised depending on the duration of the plasma pre-treatment. The cement lenses finally feature dimensions in the range of some millimetres.
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