Gas chromatography−mass spectrometry (GC−MS) and GC−tandem MS (GC−MS/MS) are useful in many separation and characterization procedures. GC−MS is now a common tool in industry and research, and increasingly, GC−MS/ MS is applied to the measurement of trace components in complex mixtures. This report describes an upper-level undergraduate experiment to understand aspects of GC−MS analysis for a mixture of compounds, carry out a protocol for selected ion monitoring, and then determine a number of kerosene component classes using GC−MS. The first exercise analyzes a standard solution containing different compounds by using GC−MS, obtains characteristic ions, conducts library searching, calculates retention indices, and displays various extracted ion plots. Selected ion monitoring is then conducted based on retention time windows and characteristic ions for this sample. Kerosene is then analyzed by GC−MS to identify various classes of compounds using extracted ion plots to support compound class monitoring. The methods described in this report may be readily adapted to other kerosene components and other samples such as pesticides, essential oils, or other samples of interest.
Magnetic stirrers and hot plates
are key components of science
laboratories. However, these are not readily available in many developing
countries due to their high cost. This article describes the design
of a low-cost magnetic stirrer with hot plate from recycled materials.
Some of the materials used are neodymium magnets and CPU fans from
discarded computers and recycled electrical components from old circuit
boards. This prototype was compared with a commercial magnetic stirrer
with hot plate. It was noted that high temperatures were reached at
similar rates, and the stirring speed was also comparable between
the two. With this prototype, which costs 80% less than commercials
ones, magnetic stirrers with hot plate can be readily available to
enhance teaching and learning in science laboratories that need them
most.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.