A novel thermal treatment, rapid transformation annealing (RTA), has been applied to six different cold rolled low-carbon (LC) steel sheets with the aim of refining their microstructure. The process involves rapid heating to just above the austenite (g) to ferrite (a) transformation temperature and subsequent rapid cooling to room temperature. Grain sizes around 2 µm in two different Nb-Ti HSLA steels, 5 µm in a Ti-LC steel and 6 µm in a plain LC (0.037%C) steel have been produced using fast cooling rates (200°C/s). Non-equiaxed structures are obtained in a Nb-Ti HSIF steel and in a plain LC (0.135%C) (CM) steel due to their higher Mn content. However, very fine equiaxed grains (2 µm) are obtained by rapid intercritical annealing (RIA) in the CM steel. Irrespective of the microalloying concept, the grain growth of recrystallized a grains before their transformation was inhibited in CM and in both HSLA steels. This inhibition is connected with the overlapping of a recrystallization and a-g transformation processes which is essential in order to achieve extreme grain refinement either by RTA or RIA.
In order to optimize the batch annealing cycles and increase the productivity of this process, the impact of the chemical composition and the processing parameters on the recrystallisation and grain growth kinetics were investigated on different Ti IF steels. A simple model based on an Avrami formulation has been developed for the prediction of the recrystallisation kinetics.
The potentialities of using the magnetic Barkhausen noise measurement in characterization of metallurgical transformations have been highlighted in multi-phase High Strength (HS) steels. This kind of steels are composed of different metallurgical constituents, such as ferrite, bainite, martensite or residual austenite. Recently, we found that it was possible to assess the proportion of phases in ferrite-martensite steels and in industrial Dual-Phase steels too. In this work, we show that the Barkhausen noise measurements can be also suitable to follow bainitic transformation in a TRIP steel.
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