The microstructural distribution associated with a hardness profile in a friction-stir-welded, agehardenable 6063 aluminum alloy has been characterized by transmission electron microscopy (TEM) and orientation imaging microscopy (OIM). The friction-stir process produces a softened region in the 6063 Al weld. Frictional heating and plastic flow during friction-stir welding create fine recrystallized grains in the weld zone and recovered grains in the thermomechanically affected zone. The hardness profile depends greatly on the precipitate distribution and only slightly on the grain size. The softened region is characterized by dissolution and growth of the precipitates during the welding. Simulated weld thermal cycles with different peak temperatures have shown that the precipitates are dissolved at temperatures higher than 675 K and that the density of the strengthening precipitate was reduced by thermal cycles lower than 675 K. A comparison between the thermal cycles and isothermal aging has suggested precipitation sequences in the softened region during friction-stir welding.
The aluminum (Al) alloys 6063-T5 and T4 were friction-stir welded at different tool rotation speeds (R), and then distributions of the microstructure and hardness were examined in these welds. The maximum temperature of the welding thermal cycle rose with increasing R values. The recrystallized grain size of the weld increased exponentially with increasing maximum temperature. The relationship between the grain size and the maximum temperature satisfied the static grain-growth equation. In the as-welded condition, 6063-T5 Al was softened around the weld center, whereas 6063-T4 Al showed homogeneous hardness profiles. Different R values did not result in significant differences in the hardness profile in these welds, except for the width of the softened region in the weld of 6063-T5 Al. Postweld aging raised the hardness in most parts of the welds, but the increase in hardness was small in the stir zone produced at the lower R values. Transmission electron microscope (TEM) observations detected a similar distribution of the strengthening precipitates in the grain interiors and the presence of a precipitation-free zone (PFZ) adjacent to the grain boundaries in all the welds. Microstructural analyses suggested that the small increase in hardness in the stir zone produced at the lower R values was caused by an increase in the volume fraction of PFZs.
The microtextures in a friction-stir-welded magnesium (Mg) alloy, AZ61, with a nugget-shaped stir zone were analyzed by orientation imaging microscopy (OIM). The base material had a (0002) ͗uvi0͘ texture ((0002) parallel to the sheet plane, ͗uvi0͘ parallel to the welding direction). Friction stir welding produced texture components different from those of the base material in the stir zone. Except for the upper surface of the plate, most of the stir zone had a texture with a strong tendency for the (0002) basal plane to align with the surface of the hard pin of the welding tool. Formation of this texture component was attributable to shear deformation arising from the rotation of the hard pin. The (0002) planes tended to align with an ellipsoidal surface in the nugget-shaped stir zone. The present study suggests that the nugget shape, which is a characteristic feature of the stir zone, is strongly related to formation of the ellipsoidal surface described by the (0002) basal plane.
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