The objectives of the study are to obtain optimum yield of extraction red rice bran oil, to determine the physico-chemical characteristics, and componen coumpounds. Data was analyzed using Nir Parametric Statistics by Friedmann test. The result showed the optimum extraction results was obtained by the ratio of substrate : solvent of 1: 8 and the oil yield was 12.31 ± 0.325%. The physico properties of red rice bran oil were greenish brown colour, with a density ranged from 0.908 ± 0.014 to 0.922 ± 0.014 (g/mL), and the water content ranged from 0.87 ± 0.06 to 0.91 ± 0.02 %. The chemical properties of red rice bran oil were: the acid number ranged from 116.41 ± 1.22 to 118.11 ± 2.45 (mg NaOH/g); the saponification number ranged from 193.74 ± 21.88 to 199.62 ± 12.63 (mg KOH/g); and the peroxide number ranged from 24.37 ± 2.44 to 26.07 ± 4.88 (mgek/kg), respectively. Oils was analyzed used GC-MS. The chemical components of rice bran oil are oleic acid (46.24%), palmitic acid (18.25%), linoleic acid (13.29%), 9-octadecane (7.76%).Key Words: Red Rice Bran, Red Rice Bran Oil, Physico-Chemical Properties, GC-MS, ChemicalCompounds. ABSTRAKTujuan penelitian untuk memperoleh rendemen optimal minyak bekatul beras merah, menentukan karakteristik fisiko kimiawi, dan komposisi kimiawinya. Data dianalisis menggunakan Statistik Nir Parametrik dengan uji Friedmann. Hasil penelitian menunjukkan hasil ekstraksi optimal diperoleh pada nisbah bahan : pelarut sebesar 1 : 8 dengan hasil rendemen minyak sebesar 12,31 ± 0,325%. Sifat fisikawi hasil minyak bekatul beras merah adalah berwarna coklat kehijauan, dengan massa jenis berkisar 0,908 ± 0,014 -0,922 ± 0,014 (g/mL), dan kadar air berkisar 0,87 ± 0,06 -0,91 ± 0,02 %. Sedangkan sifat kimiawi hasil minyak bekatul beras merah adalah sebagai berikut: bilangan asam berkisar 116,41 ± 1,22 -118,11 ± 2,45 (mg NaOH/g); bilangan penyabunan berkisar 193,74 ± 21,88 -199,62 ± 12,63 (mg KOH/g); dan bilangan peroksida berkisar 24,37 ± 2,44 -26,07 ± 4,88 (mgek/kg). Minyak dianalisis dengan menggunakan GC-MS. Komponen kimiawi penyusun minyak bekatul adalah asam oleat (46,24%), asam palmitat (18,25%), asam linoleat (13,29%), 9-oktadekenal (7,76%).