The optimum design of a die shape for Pilger mill process was carried out using FEM analyses considering various processing factors. The important design parameters of the Pilger mill machine are feed rate and profile of the grooved die. Optimum design procedure was conducted in order to investigate effects on forming load and the deformed shape of a material depending on the die surface profiles. Profiles of the die surface for the optimum design were testified with linear, cosine and quadratic curves considering physical forming process. The results of the analyses provided that the model of the quadratic profile gave the lowest forming load and the proper deformed shape.
Reducing the particle size of drug materials down to submicron is an important matter in pharmaceutical industry. Cryogenic milling technology is one of the mechanical milling processes, which is mostly utilized in refining grain size of metal and ceramics at extremely low temperature environment. This technique has not been readily studied in application to medical and biotechnology. This paper, therefore, describes the application of cryogenic milling process to reduce particle size of Ibuprofen. The shape and size of the Ibuprofen particle before and after the cryogenic ball milling process were analyzed. XRD analysis was performed to examine a change in crystallinity of Ibuprofen by the cryogenic ball milling process. The results showed that the size of Ibuprofen particles was reduced to 1/10 or less of its initial size. The results also showed that the degree of crystallinity of Ibuprofen was slightly reduced after cryogenic ball milling with nitrogen.
Multi-filament fabrication process using repetitive hydrostatic extrusion of Cu/Al at high temperature was conducted to obtain micro-scaled Aluminum wires. In the process an aluminum rod claded with a copper tube was extruded repetitively three times where a number of the single extruded rods were bundled together and subjected to hydrostatic extrusion to obtain multi-filament wire bundle. Aafter final bundle extrusion the diameter of the aluminum rod was effectively reduced from 33.6 mm to 30μm.
AZO (Aluminum doped Zinc Oxide) is widely used to produce transparent conductive coatings for liquid crystal displays, flat panel displays, plasma displays, touch panels, and electronic ink applications. The densification behavior of AZO powder is a critical factor related to the design of the compaction process. In this study, the densification behavior of AZO powder during cold compaction has been investigated in order to calibrate the modified Drucker-Prager Cap (DPC) model for FE simulations. A compaction test with a cylindrical die was carried out, and two failure tests were performed: the diameteral compression test and the uniaxial compression test. AZO compacts with various densities from the compact tests were used as specimens for the failure tests. Based on the experimental results, the parameters of the modified DPC model were determined through simple manipulations.
Adapters are a component of the output system in the internally geared hub for a bicycle. Originally, adapter parts were produced by a machining process with low productivity and material usage rate. In this study, the metal powder injection molding (MIM) process has been applied as an alternative manufacturing method to the machining process. Microstructure analysis and mechanical property testing has been conducted in order to select the material for the adapter with changes in the nickel content. The geometrical precision of the adapter is measured by using three-dimensional scanner with various mixing ratios of the powder and the binder. The developed alternative process for the adapter results in increased productivity and material usage rate. Previously, this process was only used for small parts less than 10 mm in diameter. With this development, the MIM process may be used more widely than before.
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