Here we report the catalytic oxidation of benzylic alcohol, hetero-aryl alcohols and propargylic alcohols to their corresponding carbonyl compound using heterobimetallic sodium-dioxidovanadium(V) complexes. The present catalytic oxidation studies proceed at 70°C using H 2 O 2 as terminal oxidant. During the whole process, the complexes react with hydrogen peroxide to form peroxovanadium(V) species. The present study shows the heterogeneity of pre-catalyst which could be easily recovered and moreover isolation of product is very simple.

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