The effect of power level on the microwave heating characteristics of a variety of reagent-grade chemicals and minerals has been determined in a Bureau of Mines study.Heating rates of the powdered samples are presented for incident power ranging from 500 to 2,000 W at 2.45 GHz.The apparatus consisted of a WR 975 waveguide-applicator mounted to WR 284 waveguide sections and connected to a 3-kW power source.Tests were conducted in an alumina crucible enclosed in a fused-quartz beaker that was fitted with a TeflonI lid to allow for a controlled inert atmosphere and thermocouple insertion.In general, heating rates increased as input power increased. Exceptions to this were some very high-lossy (microwave receptive) and very low-lossy materials that showed negligible changes with increased power. Microwave data collected should provide insight as to possible chemical and mineral processing applications as well as to assist in predictions of processing parameters.
The Bureau of Mines, U.S. Department of the Interior, has conducted studies to utilize rapid microwave heating to stress fracture ore samples. Iron ores containing hematite, magnetite, and goethite were subjected to microwave energy in batch operations at 3 kW and heated to average temperatures between 840° and 940° C. Scanning electron microscope (SEM) photomicrographs verified fracturing along grain boundaries and throughout the gangue matrix. Standard Bond grindability tests showed that microwave heating reduced the work index of iron ores by 9.9 to 23.7 pct. Preliminary studies using a continuous feed belt in a microwave applicator indicated that samples heat more uniformly and with better temperature control than in batch operations.
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