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A promising storage medium for hydrogen and other gases is a graphene oxide framework (GOF) that consists of layers of GO connected by benzene‐1,4‐diboronic acid (B14DBA) pillars (see picture). Theoretical predictions and the initial experimental results are presented for this cheap and environmentally friendly building block for nanoporous materials with better gas adsorption properties.

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We report the synthesis of a range of high surface area graphene oxide derived carbons (GODCs) and their applications toward carbon capture and methane storage. We obtain largely increased surface areas up to nearly 1900 m 2 g À1 for GODC samples from 10 m 2 g À1 of precursor graphene oxide (GO). Our GODCs reveal favourable gas adsorption capacities compared to other high surface area carbons. We show that producing high surface area carbons from GO precursor is a viable method, and the porosity parameters are easily tuneable for their potential gas adsorption applications.