Based on SPME‐GC‐MS analysis, it could be found that the production of acetic acid, phenethyl acetate, and isoamyl acetate gradually increased in the apple vinegar fermentation broth with the fermentation time. Consequently, in order to systematically explore the dynamic changes of microbial diversity and metabolites in the process of apple vinegar fermentation, 16S rDNA were sequenced and analyzed in this work. The present results showed that bacterial diversity was rich and exhibited a certain variation during the dynamic fermentation process of apple vinegar. Furthermore, Lactococcus and Oenococcus were the predominant bacteria in the pre‐fermentation (alcoholic fermentation) of apple vinegar, while the dominant bacteria in the middle and late fermentation stages (acetic acid fermentation) were Lactococcus and Acetobacter . In addition, during the whole fermentation process of apple vinegar, Lactococcus was the most dominant bacteria, Oenococcus was the unique species in the stage of alcohol fermentation, and Acetobacter increased rapidly in the stage of acetic acid fermentation. In conclusion, our finding provided a theoretical basis for the processing technology of apple vinegar fermentation, and a theory evidence for the safety and health assessment of apple vinegar.

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Boron carbide (B4C) possesses unique physical and thermal properties. In this paper, B4C based composites toughened by TiB2 were fabricated by in-situ reaction sintering with the original microcrystalline powders B4C, TiO2 and glucose. The influences of sintering temperature and content of TiO2 on the sintering behavior and mechanical properties were investigated. (TiB2, Al2O3)/B4C and (TiB2,SiC)/B4C composites with almost fully dense were fabricated by using additives　of Al2O3 and Si powders and sintering at 1950°C and 1900°C, the fracture toughness of composites reach to 7.09 and 6.35 MPa•m1/2 respectively. The analysis of microstructure shows that the main toughen mechanism is the crack deflection due to the existence of residual stress.

Aiming at the development of remaining oil after polymer flooding, the author develops an oil displacement technology, alternately injecting the slug of the gel and polymer/surfactant compound system, which can advanced improve the remained oil after polymer flooding. By using the artificial large flat-panel model, the oil displacement experiments are carried on to study the injection characteristics and the displacement efficiency of the alternately injecting the slug of gel and polymer/surfactant compound system, and whether the following water should be injected after polymer flooding has been discussed. The experimental results show that, the recovery of alternately injecting the gel and polymer/surfactant slug after polymer flooding could enhance recovery more than 10% on the basis of polymer flooding, the following water after polymer flooding has a little impact on the final recovery but increasing time and the difficulty of development. Therefore, these results provide the technology that alternately injecting the slug of the gel and polymer/surfactant could advance develop the residual oil and enhance the recovery after polymer flooding.

At present, the research on the performance of the shear and durability of CFRP reinforced concrete beams is few, the destruction of the curved and scissor section is often much subtle and suddenly. Based on the experimental investigation on the durableness of the CFRP concrete beams which has been shear reinforced and non-reinforced in the chloride ion erode, a comparative analysis on the fissure development, deflection, electrochemistry index and strain of the concrete beam were given under load. The results indicate that carbon fiber could limit the fissure development efficiently, and there were not the shear failure after loading, the beams with carbon could improve its shear capacity and durability efficiently, But The increase of durability is more depends on the reinforcement way.