This paper deals with the investigation of complex corrosion properties of 3D printed AISI 316L steel and the influence of additional heat treatment on the resulting corrosion and mechanical parameters. There was an isotonic solution used for the simulation of the human body and a diluted sulfuric acid solution for the study of intergranular corrosion damage of the tested samples. There were significant microstructural changes found for each type of heat treatment at 650 and 1050 °C, which resulted in different corrosion properties of the tested samples. There were changes of corrosion potential, corrosion rate and polarization resistance found by the potentiodynamic polarization method. With regard to these results, the most appropriate heat treatment can be applied to applications with intended use in medicine.
The contribution is aimed at corrosion propertied and wettability of basic graded of stainless steel commonly used in medicine as a standard for construction of instruments and other applications. Samples of AISI 304 (1.4301) steel were chemical passivated by nitric acid and tested for corrosion resistance in environment of sodium hypochlorite (NaClO), which is commonly used for basic disinfection of surfaces or devices in hospital facilities. It was found that chemical passivation of stainless steel surface increases its corrosion resistance and lower corrosion rate. Passivation layer also shows more polarization resistance. The wettability of passivated surface was measured by sessile drop method. Wettability itself determinates effectivity of disinfection process as the surfaces with lower contact angle may be cleaned and disinfected with more efficiency. It was proofed that chemical passivation increases wettability by lowering contact angle of treated surface.
In this paper corrosion properties and microstructure features of amorphous self-organised TiO2 nanotubes electrochemically deposited on titanium are discussed. There was titanium of second grade used as a substrate for these experiments. There was a specific solution of ammonium fluoride, ethylenglycol and deionized water used to create an oxide layer with advantageous properties. Relation between changes of roughness indexes before and after anodization was found out. The wettability (contact angle) of artificial plasma on surface was measured using sessile drop method. It was found out that titanium dioxide nanotubes formed on the surface significantly decreases contact angle and time of anodization reduces it even more. Corrosion potentials, corrosion rate or polarization resistance were determined by linear polarization methods performed by ASTM standards. Corrosion potential of anodized samples is substantially more positive (≈ -50mV) compared with non-treated sample (≈ -280mV). On the other hand polarization resistance was significantly higher for non-treated sample. Also potentials of passive layer breakdowns were found. Structure of nanotubes and influence of anodization on surface profile was studied by SEM.
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