In this work was investigated the microstructural evolution process of the duplex stainless steel SAF 2205 as-cast after solution annealing treatment. The aim was to detect the effects on the material microstructure by the cooling rate variation. The studied material were submitted to solution anneal at 1100 °C for 240 min, followed by cooling in water, air and furnace. The results evaluation was based on micrographic analysis, energy dispersive spectrometry measurements (EDS), X-ray diffraction and hardness tests. The ferrite volume fraction obtained in the microstructure increased with the cooling rate, because it causes diffusion inhibition of the steel constituent elements, promoting retention of the ferrite. The volume fraction of austenite phase increased with a lower cooling rate. The cooling rate is an important factor in defining the steel microstructure, particularly about intermetallic phases precipitation, which occurred by the slow cooling rate. Additionally, it was observed the precipitation of sigma phase.
Titanium and stainless steel are examples of biomaterials widely used in dental and orthopedic implants owing to their properties of good corrosion resistance and excellent biocompatibility. This paper reports on a study of the biomimetic method applied to titanium (cp-Ti) and 316L stainless steel. The method consists in immersing the metal substrate in a synthetic solution of SBF (simulated body fluid) whose composition, pH and temperature resemble those of human blood plasma. The coating on the two metals was effective for obtaining hydroxyapatite, which was confirmed by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR).
The difficulties experienced in welding processes of martensitic stainless steel led to development of a new class of them, known as stainless mild martensitic steels. Also, due to the current high demand for energy and materials to oil extraction at great depths, scientists have being developing specific researches about mechanical resistance and corrosion of steels and how these properties are influenced by high temperature processes. This research studies the effect of welding process over the corrosion resistance of the 13Cr4Ni0.02C steel in a lithium chloride solution with a concentration of 120,000 PPM Cl-. The corrosion tests were conducted by cyclic potentiodynamic polarization in the base metal, weld bead and heat affected zone (HAZ) areas of the steel, in average temperatures of 23°C (as reference) and 3°C. The results revealed that the weld bead and heat affected zones of the 13Cr4Ni0.02C steel in a temperature of 3°C are less resistant to corrosion in this environment than the base metal in the same conditions.
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