To improve fracture toughness and encourage excellent self‐crack‐healing ability, mullite/SiC particle/SiC whisker multi‐composites and mullite/SiC whisker composites were hot pressed. The crack‐healing abilities and mechanical properties of these sintered composites were investigated. Based on the obtained results, the usefulness of the mullite composite as a material for springs was discussed. The part of mullite/15 vol% SiC whisker/SiC 10 vol% particle containing healed cracks retained high reliability over the whole measured temperature range. When the crack‐healing ability was endowed by SiC whiskers alone, the parts containing the healed pre‐cracks were found to have a heat‐resistance limit temperature. Mullite/15 vol% SiC whisker/10 vol% SiC particle multi‐composite had the best potential as a material for springs used at high temperatures, because it had an adequate crack‐healing ability as well as shear deformation ability almost two times stronger than that of monolithic mullite.
Within session and between session reliabilities of the task-related component (P3b) of the P3 measures (amplitude, area and latency) and their habituation across eight sessions separated by 7-10 days, except for an interval of 1 month between the 6th and 7th sessions, were studied based on the difference waves, which were obtained by subtracting the ignored infrequent event-related potentials (ERP) from the target ERP elicited by a standard auditory oddball paradigm with eyes-open or eyes-closed conditions in 10 normal subjects. The within session reliabilities represented as Pearson correlation coefficients (r) were 0.57-0.66 for the three measures except for those for the latency and amplitude under the eyes-closed condition. The between session reliabilities expressed as intraclass correlation coefficients (R) ranged from 0.54 to 0.60 except for that for latency under eyes-closed conditions. Long-term habituation occurred within the first six sessions for the P3b amplitude and area, and dishabituation took place in the 7th session after an interval of 1 month, whereas no such phenomenon was observed for the P3b latency. Implications of the present results are discussed in terms of the clinical application of the P3 measures.
Fatigue properties in high pressure gaseous hydrogen environment were investigated for pipe materials used in fuel cell vehicles and hydrogen stations. Cyclic pressurization tests were conducted using a tubular specimen filled with hydrogen pressurized up to 90MPa. Tested materials were types 316L, 304 and A286 stainless steels, low alloy steels such as JIS SCM435 (1.0Cr-0.2Mo), Cr-Mo-V steels. The fatigue life in hydrogen was compared with that in inert gas to evaluate the effect of gaseous hydrogen on fatigue properties. The fatigue life in hydrogen was slightly shorter than that in argon in the case of a stable stainless steel type 316L. In contrast, a metastable stainless steel type 304 showed a remarkable degradation of the fatigue life in the hydrogen environment. Although the fatigue lives in hydrogen of type 316L and 304 stainless steels decreased with the increase in the cycle times, the fatigue lives remained unchanged over 10 2 of the cycle time. The fatigue life of low alloy SCM435 steel in hydrogen extremely decreased. The fatigue life of high-strength austenitic steel A286 in hydrogen is much better than that of low alloy SCM435 steel at the same tensile strength. The Cr-Mo-V steels showed longer fatigue lives than JIS SCM 435 at same strength levels in hydrogen. Fracture surfaces revealed transgranular cracking for the Cr-Mo-V steels, while intergranular cracking was observed for SCM435 with tensile strength more than 1.2GPa. It was assumed that the carbide precipitation affected the fracture morphology.
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