Durch Umsetzung von Boc‐Lys(Z)‐Thr‐Lys(Z)‐Thr‐N3 [3] mit Lys(Z)‐Lys(Z)‐D‐Leu OMe [1] wird das Heptapeptid Boc‐Lys(Z)‐Thr‐Lys(Z)‐Thr‐Lys(Z)‐Lys(Z)‐D‐Leu‐OMe 13 erhalten. Nach Abspaltung der Boc‐Gruppe wird es mit dem Tripeptid‐Derivat Boc‐Ile‐Lys(Z)‐Lys(Pht)‐ONP 7 zum vollständig geschützten Dekapeptid Boc‐Ile ‐Lys(Z)‐Lys(Pht)‐Lys(Z)‐Thr‐Lys(Z)‐Thr‐Lys (Z)‐Lys(Z)‐D‐Leu‐OMe 14 umgesetzt.
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