The objective of this study was to investigate the mechanical properties of wood/plastic composites (WPCs) produced using wood flour (WF) prepared by wet ball-milling under various milling times (0-120 min) and drying methods (freeze-or heat drying). The drying method did not affect the particle size distribution, shape, or specific surface area of WF at milling times shorter than 40 min. At milling ≥ 40 min, freeze-dried ball-milled WF (FDWF) had smaller particle sizes and higher specific surface area than heat-dried ball-milled WF (HDWF). The highest tensile strength and modulus of rupture (MOR) were observed in WPCs made from freeze-and heat-dried WF at a milling time of 30 min. At milling time of 30 min, the amount of 100-300 µm FDWF and HDWF was 37% and 36%, respectively. The impact strength of WPCs increased, as the milling time increased. The amount of small freeze-and heat-dried WF particles increased due to an increase in the amount of 17 µm particles and specific surface area with increased milling time. Thus, impact strength of WPCs increased as particle size decreased. At milling times ≤ 60 min, there were no significant differences in mechanical properties between WPCs containing freeze-and heat-dried WF under the condition of this study.
The aim of this study was to investigate the effect of impregnating materials (low molecular weight phenol formaldehyde or LmwPF and succinic anhydride or SA), their concentrations (5and 10%), and compression ratios (20 and 40% from initial thickness)on improvement of specific gravity (SG) and dimensional stability on nyatoh, sepetir, and pisang putih wood; and then compared them to control and densified wood. The results showed that SG and dimensional stability of compregnated wood were affected by all parameters studied. Higher compression ratio and concentration will result in a greater improvement.In general, SG and dimensional stability of compregnated wood were better than the control.SG of LmwPF-and SA-compregnated wood increased by 10.69‒22.31% and 6.96‒23.09%, respectively. Utilization of LmwPF and SA has significantly reduced the spring-back, butthe latter is better. Thecompression-set recovery after compregnation was 18.34‒33.99%, while after densification was 47.86‒71.49%.
The addition of maleic anhydride (MA)-modified polypropylene (MAPP) as a compatibilizer increases mechanical and physical properties of wood/plastic composites (WPCs). It is thought that MA graft ratio (Gr), molecular weight (weight-average molecular weight [Mw]), and mixing methods of MAPP affect physical and mechanical properties of WPCs. However, evaluation, especially for mixing order, is not enough. The objective of this study was to investigate the effect of Gr and Mw of MAPP and its mixing methods on the mechanical and physical properties of WPCs. Two types of mixing methods were used: mixing the MAPP with the filler using a Henschel mixer before kneading with PP (premixing method) and mixing all of the materials at one time (one-step mixing method). The WPCs made with the premixing method had lower shear viscosity and higher flexural modulus than those made with the one-step mixing method. The particle size, moisture content, and surface morphology of fillers are thought to be more important in determining the shear viscosity of WPCs than the MAPP itself. The highest tensile, impact, and flexural strengths of WPCs were obtained in the WPC with premixing with low-Gr and high-Mw MAPP. It may be due to the effective reaction of the wood flour with MAPP and higher entanglement between the MAPP and PP. These results suggest that the premixing method could improve productivity and mechanical properties of WPCs.
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