Tomographic measurement techniques offer the opportunity to quantify the degree of homogeneity of particulate suspensions and other multiphase mixtures. Electrical resistance tomography is a relatively simple and inexpensive technique for measuring the distribution of electrical conductivity within multiphase systems. This can provide pertinent information about the physical form, the chemical composition, or the general status of manufacturing. In this contribution, we present recent applications of this technology to processes in pharmaceutical and related application areas. Examples include on-line measurement of solids distribution in stirred tanks and crystallizers, monitoring the performance of an industrial pressure filter, and flow profile and velocity measurements in a physical model of a catalytic reactor.
This paper reports the performance of a research prototype of a new multiphase flow instrument to non-invasively measure the phase flow rates, with the capability to rapidly image the flow distributions of two-(solids, gas or oil in water) and three-phase (gas and oil in water) flows. The research prototype is based on the novel concepts of combining vector Electrical Impedance Tomography (EIT) sensor (for measuring dispersed-phase velocity and fraction) with an electromagnetic flow meter (EMF, for measuring continuous-phase velocity with the EIT input) and a gradiomanometer flowmixture density meter (FDM), in addition to on-line water conductivity, temperature and absolute pressure measurements. EIT-EMF-FDM data fusion embedded in the research prototype, including online calibration of reference conductivity and online compensation of conductivity change due to the change of fluids' temperature or ionic concentration, enables the determination of mean concentration, mean velocity and hence the mean flow rate of each individual phase based on the measurement of dispersed-phase distributions and velocity profiles. Results from recent flow-loop experiments at Schlumberger Gould Research (SGR) will be described. The performance of the research prototype in flow-rate measurements are evaluated by comparison with the flow-loop references. The results indicate that optimum performance of the research prototype for three-phase flows is confined within the measuring envelope 45%-100% WLR and 0%-45% GVF, which is the sweet point of the measurement system. Within the scope of this joint research project funded by the UK Engineering & Physical Sciences Research Council (EPSRC), only vertical flows with a conductive continuous liquid phase will be addressed.
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