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Black silicon and its application as a new assembly method for silicon wafers at room temperature is presented. Needle-like structures on the surface after deep reactive ion etching with a length of 15–25 µm and 300–500 nm in diameter interlock with each other to form a bonding interface. After compression of two wafers at room temperature they generate retention forces up to 380 N cm−2 (3.8 MPa). If low contact forces are applied with partially interlocking of the needles, it is possible to generate a reversible Velcro®-like assembly. This new bonding process can be used for applications in the area of microfluidics with catalysts, microoptical or mechanical mountings or carrier wafer bonding in microelectronics.

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ABSTRACT--A novel dynamic friction experiment using the Kolsky bar concept was developed. The technique is complementary to the plate impact and other macroscopic friction experiments in the sense that sliding velocities and pressures not attainable otherwise can be investigated. The experimental results reported in this article show that the technique provides accurate and repeatable measurement of time-resolved friction. The apparatus is simpler and easier to operate than the plate impact facility. However, it cannot achieve the same level of contact pressure. Several material pairs have been investigated. In particular, the kinetic friction coefficient of Ti-6AI-4V sliding against WC/Co (cerrmet) and 4340 steel sliding against WC/Co were measured and compared with the values reported by Prakash and Clifton in 1993. Atomic force microscopy is used to characterize the surface topography before and after the friction tests.

Comprehensive multi-dimensional hyphenation of a thermogravimetry device (i.e. a thermobalance) to gas chromatography and single photon ionization-time-of-flight mass spectrometry (TG-GC×SPI-MS) has been used to investigate two crude oil samples of different geographical origin. The source of the applied vacuum ultraviolet radiation is an electron beam pumped rare gas excimer lamp (EBEL). The soft photoionization favors the formation of molecular ions. Introduction of a fast, rapidly modulated gas chromatographic separation step in comparison with solely TG-SPI-MS enables strongly enhanced detection especially with such highly complex organic matrices as crude oil. In contrast with former TG-SPI-MS measurements, separation and identification of overlying substances is possible because of different GC retention times. The specific contribution of isobaric compounds to one mass signal is determined for alkanes, naphthalenes, alkylated benzenes, and other compounds.