Using a vacuum during the smelting and refining of alloys removes dissolved gasses, as well as impurities with high vapour pressure. When smelting is carried out in vacuum induction furnaces, the intensification of the discussed processes is achieved by intensive mixing of the bath, as well as an enhanced mass exchange surface (liquid metal surface) due to the formation of a meniscus. This is due to the electromagnetic field applied to the liquid metal. This study reports the removal of zinc from the Al-Zn alloy containing 6.3 wt.%. Zn. The experiments were carried out with the use of two types of metallurgical devices: the VIM and ISM furnaces. For the experiments carried out in the crucible induction furnace, reduction in the operating pressure in the furnace from 1000 Pa to 10 Pa, together with the increase in temperature from 953 K to 1103 K, is accompanied by a decrease in zinc content in the alloy from 6 to 96%, compared with the initial value. Simultaneously, the overall mass transfer coefficient kZn increases from 5.15 × 10−6 to −1.49 × 10−4 ms−1. For the experiments carried out in the furnace with a cold crucible (T = 953 K), a reduction in the operating pressure in the furnace from 1000 Pa to 10 Pa resulted in a decrease in zinc content in the alloy from 18 to 80%, compared with the initial value. For comparison, the experiments carried out in the crucible induction furnace at 953 K showed a reduction in zinc content in the alloy from 6 to 50%, which means that more intense zinc evaporation is seen in the furnace with a cold crucible. Comparison of ISM and VIM technologies in the removal efficiency of the Al-Zn alloy indicates a higher removal efficiency using the first technology, which, using the same conditions, achieves 80% of the removal efficiency of the component.
Innovative technologies require the use of materials that meet increasingly high requirements; one such requirement is the purity of metals. In the case of copper, this translates into a parameter related to electrical conductivity. Traditional metal refining technologies have some limitations that can be eliminated through the use of modern melting aggregates. Such solutions include vacuum induction furnaces, comprising an induction furnace with a cold crucible. As part of this work, the possibilities of refining copper and lead alloys were investigated. In addition, the research was carried out with the use of two induction vacuum aggregates, allowing us to compare their effectiveness. The tests were carried out in a pressure range of 10–1000 Pa and at temperatures of 1273–1473 K. The results obtained made it possible to determine the mass transport coefficient of lead from an alloy with copper, and to determine the share of resistance in individual stages of the process. For experiments conducted inside an induction crucible furnace, lowering the working pressure inside the furnace chamber from 1000 to 10 Pa while increasing the temperature from 1323 to 1473 K was accompanied by a drop in the lead concentration inside the alloy of 69 to 96%, compared to its initial mass. For experiments conducted inside a cold crucible furnace, approximate values of lead removal appeared for lower temperatures (1273 to 1323 K), confirming that the analyzed process happens faster in this aggregate.
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