This work presents the employment of a frequently-used ultrafiltration technique to drastically reduce the time required for the synthesis of chitosan nanowires, iron oxide nanowires and their complex nanowires. Instead of synthesizing iron oxide nanowires using time-consuming template and hydrothermal methods, a centrifugation force provides a tangential flow to force both iron ions and/or the diluted chitosan solution to pass through a filter and co-precipitate into nanowires within 1 min. Two parameters, centrifugation force and alkaline concentration, can directly control the diameters and lengths of nanowires. Experimental Preparation of nanowiresIron(III) chloride hexahydrate and iron(II) chloride tetrahydrate were purchased from Merck Co. and used as received. Iron oxide

In this study, a morphological diagram was constructed for quantitatively predicting various modes of surface instabilities caused by the dynamic interfacial release of strain in initially flat bilayer composites comprising an elastomer and a capping layer. Theory, experiment, and simulation were combined to produce the diagram, which enables systematic generation of the following instability patterns: wrinkle, fold, period-double, delamination, and coexisting patterns. The pattern that forms is most strongly affected by three experimental parameters: the elastic modulus of the elastomer, the elastic modulus of the capping layer, and the thickness of the capping layer. The morphological diagram offers understanding of the formation of complex patterns and development of their applications. Critically, the wrinkle alignment can be well controlled by changing the direction of the interfacial release to enable the creation of centimeter-sized and highly ordered lamellar wrinkled patterns with a single orientation on a soft elastomer without the need for costly high-vacuum instruments or complex fabrication processes. The method and diagram have great potential for broad use in many practical applications ranging from flexible electronic devices to smart windows.