Crack growth in silica optical fibers was measured directly in a wide range of crack velocities da/dt (10−13 < da/dt < 10−5 m/s) by improving our previous method. The slope in log‐log plots of the crack velocity versus the stress intensity factor data was revealed to increase with the crack velocity, e.g., slope, 23.3 for da/dt < 10−10 m/s, and 39.7 for da/dt > 1(10−8 m/s. The data were also found to be fitted well by the exponential law in the whole range of da/dt, rather than the power law. Additionally, the fiber data were shown to be close to those reported for bulk silica specimens having large cracks for high crack velocities where the bulk specimens were tested.
Atomic force acoustic microscopy (AFAM) provides nanometre resolution images reflecting
sample elasticity and a possible technique for measuring the elastic modulus of thin films
and extremely narrow areas. In AFAM, the resonant frequency of a micro-cantilever
equipped with a sensor tip measures the contact stiffness between tip and sample. In
the case of stiff samples like metals and ceramics, AFAM exhibits significantly
low sensitivity, i.e., the resonant frequency is insensitive to the contact stiffness.
The proposed concentrated-mass (CM) cantilever offers a smart solution to the
problem without trade-offs. The present study discusses schemes for imaging
elastic heterogeneity and evaluating elastic modulus in the case of CM cantilevers.
The present experiment employed a flat tip with a metallic coating, namely a
Ti/Pt thin film. The adhesive strength and ductility of the coating resulted in a
prolonged lifetime. Images of a Ti sheet sample acquired with so-called slope
detection clearly revealed nano-grains and slip bands, which would be unachievable
by topographic images. The flat tip ensures a constant contact area, rendering
contact stiffness independent of the magnitude of the contact force and tip–sample
adhesion force, and significantly simplifying evaluation of the elastic modulus.
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