Fractal dimension is a versatile method to study and evaluate corrosion from the point of view of metallic conditions, namely: surface roughness, electrochemical measurements and microscopy images. Aluminum corrodes at different rates, under different pH electrolytes with or without the presence of chloride ions. In this work, corrosion and the surface roughness for aluminum corrosion at different pH electrolytes: acid, with and without chlorides, neutral and basic solutions, were obtained. It was measured and obtained using electrochemical and optic techniques. The results of Electrochemical Impedance Spectroscopy (EIS) and Noise Measurements (ENM), Digital Holographic Microscopy (DHM), Scanning Electron Microscope (SEM) micrographs and their respective Fractal Dimension analysis were obtained.. For the different experimental techniques and conditions, fractal dimension was obtained and presented, reflecting the surface condition of aluminum corrosion as a function of pH solution.
In this work, synthesis and characterization of reduced graphene oxide/polyaniline/Au nanoparticles (GO/PANI/NpAu) as a hybrid capacitor are presented. Graphite oxide (GO) was synthesized by a modified Hummer's method. Polyaniline was synthesized by chemical polymerization, and Au nanoparticles (NpAu) were added afterward. Fabrication of the electrodes consisted on the hybrid materials being deposited on carbon cloth electrodes. The chemical and structural properties of the electrode were characterized by high-resolution scanning electron microscopy (HRSEM), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (X-R), and Raman spectroscopy; the results confirm the graphene reduction, the covalent functionalization, and formation of nanocomposites and also show the polyaniline grafted graphene. The performance and evaluation of the electrodes based on grapheme oxide (GO), polyaniline (PANI), GO-PANI, and GO/PANI/NpAu nanocomposites over carbon cloth, stainless steel, and copper have been obtained in 1 M H 2 SO 4 solution, using electrochemical techniques namely: cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS). They showed that GO/PANI/NpAu gave higher specific capacitance (SC) and energy values than PANI, and GO/PANI, in the order of 160 F/g. The present study introduces new hybrid material for energy applications, from the evaluation of their electrical contributions.
Background: :
Fractal dimension is a versatile method to study and evaluate corrosion from the point of view of metallic conditions, namely: surface roughness, electrochemical measurements and microscopy images. Aluminum corrodes at different rates, under different pH electrolytes with or without the presence of chloride ions.
Methods::
In this work, corrosion and the roughness for aluminum corrosion at different pH electrolytes: acid, with and without chlorides, neutral and basic solutions, It was measured using electrochemical and optic techniques.
Results::
The results of Electrochemical Impedance Spectroscopy (EIS) and Noise Measurements (ENM), Digital Holographic Microscopy (DHM), Scanning Electron Microscope (SEM) micrographs and their respective Fractal Dimension analysis were obtained.
Conclusions::
For the different experimental techniques and conditions, fractal dimension were presented, reflecting the surface condition of aluminum corrosion as a function of pH solution.
Fractal dimension is a versatile method to study and evaluate corrosion from the point of view of metallic conditions, namely: surface roughness, electrochemical measurements and microscopy images. Aluminum corrodes at different rates, under different pH electrolytes with or without the presence of chloride ions. In this work, corrosion and the surface roughness for aluminum corrosion at different pH electrolytes: acid, with and without chlorides, neutral and basic solutions, were obtained. It was measured and obtained using electrochemical and optic techniques. The results of Electrochemical Impedance Spectroscopy (EIS) and Noise Measurements (ENM), Digital Holographic Microscopy (DHM), Scanning Electron Microscope (SEM) micrographs and their respective Fractal Dimension analysis were obtained.. For the different experimental techniques and conditions, fractal dimension was obtained and presented, reflecting the surface condition of aluminum corrosion as a function of pH solution.
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