The present study was realized for measuring viscosities of reference liquids using capillary viscometers and Stabinger viscometer SVM 3001 with viscosity interval between 1 mm2/s and 5000 mm2/s with temperatures from 20 °C to 80 °C. Based on our measurement with various liquids, we determine the viscosity values and compare both of the results. The aim of this study to evaluate the results of the primary level viscosity measurement system and stabinger viscometer and to compare the measurement results due to the providing traceability of Stabinger viscometer by TUBITAK UME. An increasing number of national metrology institutes and accredited laboratories provide viscometer calibration with reference liquids in a wide viscosity range. It is a common practice to use the viscosity of water as the metrological basic of viscometry. The national standard of viscosity provided by TUBITAK UME consists of a set of ubbelohde viscometers covering the measuring range of kinematic viscosities from about 0.5 mm2/s to 100 000 mm2/s. At the low viscosity, long − capillary viscometers are used as primary standards which are directly calibrated water.

In this study, the determination of weighing liquid by using automatic alignment system and the reference density standard to realize the calibration of scale division by hydrostatic weighing method introduced by Cuckow in computer controll is planned. This system serves all projects of Volume, Density and Viscosity Laboratory for the calibration process of hydrometers and makes it fully automatic, fast, more precise and efficient in comparison with manual calibration system. A new method refers automatically specific scale-marks for the calibration of hydrometers. A hydrometer calibration system adopting the new method consists of a vision system, positioning frame by servo motor and software to control the system. The vision system is composed of a camera to acquire images of meniscus level conflicted with scale level of hydrometer. The position of temperature controlled bath is provided by the positioning frame controlled with PLC. The stepping motor moves the camera, which is attached to the vessel containing a reference liquid, along the hydrometer. The aim of this study is to represent and validate the automated hydrometer calibration system of TUBITAK UME realizing the hydrometer comparison (1000-1020 kg/m 3 ) between automated and manual hydrometer calibration system.

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This report describes the third CCM key comparison in capillary viscometry at twelve National Metrology Institutes (NMIs), which was carried out between October 2012 and February 2013. Seven NMIs, which do not maintain an independent viscosity scale, also took part in this comparison. Three samples of Newtonian liquids with nominal kinematic viscosities of 6 mm²/s at 15 °C and 5 mm²/s at 20 °C, 2000 mm²/s at 20 °C and 500 mm²/s at 40 °C, and 160000 mm²/s at 20 °C and 25000 mm²/s at 40 °C prepared by NMIJ were provided to each of the NMIs. For each of these liquids at two temperatures, total number of 98 measurements was carried out and from the results of viscosity measurements, the key comparison reference values (KCRVs) for six data sets were determined. The degrees of equivalences was evaluated by difference from the KCRV and, with a few exceptions, these differences were almost equal to or less than expanded uncertainties, showing a good equivalencies of capabilities at the participating NMIs for the viscosity measurements in wide range of viscosities covered from 5 mm²/s to 160000 mm²/s. KEY WORDS FOR SEARCH Main text To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/. The final report has been peer-reviewed and approved for publication by the CCM, according to the provisions of the CIPM Mutual Recognition Arrangement (CIPM MRA).