This article describes microprobes for noncontact scanning force microscopy that make use of a direct-oscillating thermally driven bimorph actuator with integrated piezoresistive readout sensor. The sensitivity has been increased using direct current for biasing and alternating current for exciting the thermally driven cantilever in a higher flexural mode. The cantilever operates in the phase-shift atomic force microscopy (AFM) detection technique. The main advantage of phase imaging is the higher z resolution at high scan rates and much lower forces than in height imaging with contact AFM. Critical dimensions measurements illustrating the imaging capability and resolution of our new scanning proximal probe are demonstrated.

Structural characterization of a fully etched amorphous W/Si multilayer grating with a lateral periodicity of 800 nm is performed by x-ray reflectivity in the coplanar and non-coplanar modes using a scintillation detector and a two-dimensional gas-filled detector, respectively. Three-dimensional reciprocal space constructions were used to explain the scattering features recorded in both geometries. Coplanar coherent grating truncation rods were fitted by a dynamical theory for rough gratings. Comparison of the reflectivity from the reference planar multilayer completes the study.

In the last years, silicon micromachining techniques based on high aspect ratio reactive ion etching with gas chopping have been developed. There the gas flow of etching and deposition gas precursors is chopped which results in controllable sidewall passivation and high anisotropy. However, the rippled sidewalls are a serious limit for various applications. We report on the development of a novel gas chopping etching technique (GCET) process in order to achieve a smooth (rippled free) sidewall surface. As the direct etch mask, we used a 1 or 2-μm-thick resist layer, which was lithographically patterned. The novelty of the process consists in the replacing of the isotropic etching step by an anisotropic etching step. In this way we omit the main source for sidewall ripples. GCET combined with inductively coupled plasmas and fluorine chemistry provide very high etch rates and good control of the sidewall slope. These techniques also can be applied to conventional reactive ion etching equipment with Cl or F based plasma chemistry. However, the techniques used in this study have lower selectivity (in range of 30) than the conventional GCET. A SiON/Si selectivity as high as 50 has been achieved.

Miniaturized viscosity sensors are often characterized by high-resonance frequencies and low-vibration amplitudes. The viscosity parameter obtained by such devices is therefore not always comparable to those probed by conventional laboratory equipment. We present a novel micromachined viscosity sensor with relatively low operating frequencies in the kHz range. The sensor utilizes Lorentz force excitation and piezoresistive readout. The resonating part consists of a rectangular plate suspended by four beam springs. The first mode of vibration is an in-plane mode. Thus, the contribution of the moving plate to the device damping is low, whereas the overall mass is high. This principle improves the quality factor and gives additional freedom to the device designer. This paper presents the device concept, the fabrication process and a prototype of the viscosity sensor. Measurement results demonstrate the feasibility of the device and show that the damping of the device is an appropriate measure for the viscosity.

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