In the present work, characterization of sintering behavior of Tungsten heavy alloy has been done through powder metallurgy route using Spark plasma sintering (SPS). Fine powder of Tungsten (<30 µm) was separately mixed with Ni, Co, Fe, Mo and Cu each with 1 weight%. Spark Plasma Sintering (SPS) technique (1200°C, 20 MPa pressure with 1 min holding time) was used to sinter the mixed powders. The maximum density was observed in W-Ni followed by Co, Fe, Cu, Mo and with least in pure tungsten sample. Optical microscopy as well SEM was done to determine the microstructure and grain coarsening. Due to the short heating time very less grain coarsening was observed. Vickers hardness test was conducted which resulted in maximum hardness in case if W-1Fe SPS sample.

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Spark plasma sintering provides faster heating that can create fully, or near fully, dense samples without significant grain growth. In this study, pre-alloyed Ti-6Al-4 V powder compact samples produced through field assisted sintering in a spark plasma sintering machine are compared as a function of consolidation temperature. The effect of sintering temperature on the densification mechanism, microstructural evolution and mechanical properties of spark plasma sintered Ti-6Al-4 V alloy compacts was investigated in detail. The compact, sintered at 1100 °C, exhibited near net density, highest hardness and strength as compared to the other compacts processed at a temperature lower than 1100 °C.