Paul A. Lovatt scite author profile

Measurements of adsorption isotherms of a series of thirteen mono- and di-phosphonic acids have shown that these bind strongly to the surface of high surface area aluminium trihydroxide. The incorporation of such phosphonates into a suspension of aluminium flake in an aqueous medium, modelling the continuous phase of a water-based paint, greatly suppresses the evolution of hydrogen. Whilst strong binding of the phosphonate to aluminium oxides is an essential criterion for good passivation, other factors such as the hydrophobicity of the ligand are also important in suppressing hydrogen-evolution.

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A general route for the synthesis of triazacyclononane functionalised with one, two or three pendant phosphine arms: crystal structure of [Zn2L2Cl3][ClO4], L =N-(diphenylphosphinopropyl)-1,4,7-triazacyclononane

Ellis¹,

Farrugia²,

Hickman³

et al. 1996

Chem. Commun.

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Paul A. Lovatt

Synthesis of a series of novel binucleating ligands based on 1,4,7-triazacyclononane and o-, m- and p-xylene: crystal structure of the μ-hydroxy-bridged dicopper(II) complex [Cu2Lm(OH)2][BPh4 ]2 [Lm = α,α′-bis (N-1,4,7-triazacyclononane)-m-xylene]

Macrocycles with a single pendant arm: synthesis of N-R-(1,4,7-triazacyclononane) [L, R = 4-but-1-ene; L′, R = 3-prop-1-ene]: Synthesis of the CuI complex [CuL]I and synthesis and crystal structure of the CII complex [CuL2][BPh4]2 and the μ-hydroxy bridged CII dimer [LCu(μ-OH)2CuL] [BPh4]2

Fixing Carbon Dioxide with Copper: Crystal Structure of [LCu(μ-C₂O₄)CuL][Ph₄B]₂ (L = N,N‘,N‘ ‘-Triallyl-1,4,7-triazacyclononane)

The binding of phosphonic acids at aluminium oxide surfaces and correlation with passivation of aluminium flake

A general route for the synthesis of triazacyclononane functionalised with one, two or three pendant phosphine arms: crystal structure of [Zn2L2Cl3][ClO4], L =N-(diphenylphosphinopropyl)-1,4,7-triazacyclononane

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Paul A. Lovatt

Synthesis of a series of novel binucleating ligands based on 1,4,7-triazacyclononane and o-, m- and p-xylene: crystal structure of the μ-hydroxy-bridged dicopper(II) complex [Cu2Lm(OH)2][BPh4 ]2 [Lm = α,α′-bis (N-1,4,7-triazacyclononane)-m-xylene]

Macrocycles with a single pendant arm: synthesis of N-R-(1,4,7-triazacyclononane) [L, R = 4-but-1-ene; L′, R = 3-prop-1-ene]: Synthesis of the CuI complex [CuL]I and synthesis and crystal structure of the CII complex [CuL2][BPh4]2 and the μ-hydroxy bridged CII dimer [LCu(μ-OH)2CuL] [BPh4]2

Fixing Carbon Dioxide with Copper: Crystal Structure of [LCu(μ-C2O4)CuL][Ph4B]2 (L = N,N‘,N‘ ‘-Triallyl-1,4,7-triazacyclononane)

The binding of phosphonic acids at aluminium oxide surfaces and correlation with passivation of aluminium flake

A general route for the synthesis of triazacyclononane functionalised with one, two or three pendant phosphine arms: crystal structure of [Zn2L2Cl3][ClO4], L =N-(diphenylphosphinopropyl)-1,4,7-triazacyclononane

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Fixing Carbon Dioxide with Copper: Crystal Structure of [LCu(μ-C₂O₄)CuL][Ph₄B]₂ (L = N,N‘,N‘ ‘-Triallyl-1,4,7-triazacyclononane)