The aim of this study was to evaluate the solubility of three types of root canal sealers in three organic solvents used in endodontics. The solubility of calcium-hydroxide-based (Sealer 26), silicon-polydimethylsiloxane-based (RoekoSeal), and zinc-oxide-eugenol based (Endofill and Intrafill) sealers was assessed in eucalyptol, xylol, orange oil, and distilled water. Eighty samples of each filling material were prepared according to the manufacturers' instructions and then divided into four groups for immersion in solvent for 2 or 10 min. The means of sealer dissolution in solvents were obtained by the difference between the original preimmersion weight and the postimmersion weight in a digital analytical scale. Data were statistically analyzed with the Student's t test, and multiple comparisons were performed with Student-Newman-Keuls. Xylol and orange oil showed similar effects, with significant solubilization (P<0.05) of the tested cements. Endofill and Sealer 26 did not show any significant difference in solubilization at the two immersion times, whereas RoekoSeal and Intrafill showed a more pronounced solubility at 10 min. The lowest levels of solubilization occurred in RoekoSeal, Sealer 26, Endofill, and Intrafill. It is concluded that xylol and orange oil presented similar solvent effects with a significant solubility of the tested cements.
The purpose of this investigation was to evaluate the microhardness of two laboratory-processed composites (Artglass; belleGlass) and two direct placement composites (Filtek Z250; Alert), after aging in distilled water. Twenty cylinders (8 mm diameter; 2 mm height) per tested material were prepared and stored in 10 ml of distilled water. Five Knoop hardness measurements were made on the surface of the specimens with a Miniload Hardness Tester under a load of 50 g for 30 s at 10 min, 24 h, 30 and 90 days. Statistical analysis was perfomed using two-way ANOVA, followed by a SNK multiple comparison test (p < 0.05). The analysis showed statistically significant difference among hardness means recorded at the different aging time and the tested materials. It may be concluded that all materials presented hydrolytic degradation due to aging in aqueous environment
Clinical RelevanceOne of the advantages reported for indirect composite restorations is the reduction of polymerization shrinkage, which could produce better marginal sealing. Although sealing of cervical enamel margins was slightly better for the indirect systems used, no difference between indirect and direct restorations was found for cervical margins in cementum/dentin. SUMMARYThis study compared microleakage between indirect composite inlays and direct composite restorations. Forty-eight standard inlay MOD cavities, with cervical margins located either in enamel or dentin, were prepared in extracted human third molars. The specimens were randomly divided into 3 groups (n=16). In the control group, the cavities were restored with the composite Filtek Z250 (3M ESPE). For the experimental groups, indirect restorations were made with the Artglass (Heraeus-Kulzer) or Belleglass HP (Kerr Laboratories) systems and cemented with the dual curing cement RelyX ARC (3M ESPE). The adhesive system Single Bond (3M ESPE) was applied on all groups. The specimens were submitted to thermolcycling, coated with nail varnish, then immersed in 2% basic fuchsine aqueous solution for 24 hours. The teeth were then sectioned and leakage scores were evaluated (40x), based on a standard ranking. Data were submitted to statistical analysis (Mann-Whitney and Kruskal-Wallis tests) with a 95% confidence level. No statistical difference was found between substrates (p=0.595), and the materials performed similarly in dentin (p=0.482). Direct restorations showed higher leakage than indirect restorations at the enamel margins (p=0.004). Within the limitations of this experimental design, overall leakage was similar between both substrates, while the indirect systems provided a better sealing than direct composites only in enamel.
With the methodology employed, microfill composite presented the lowest flexural strength, but its association with hybrid composite increased the resistance to fracture. The combination of polyethylene fiber and hybrid composite did not present higher flexural strength than hybrid composite alone.
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